EPA 1613 Polychlorinated Dibenzofurans Order Items Used in This Application7KG-G010-11 Zebron ZB-5MS, GC Cap. Column 60 m x 0.25 mm x 0.25 µm, Ea GC Conditions Official Method: | EPA 1613 | Column: | Zebron ZB-5MS, GC Cap. Column 60 m x 0.25 mm x 0.25 µm, Ea | Part No: | 7KG-G010-11 | | Phase Name: | ZB-5MS | Injection: | Splitless @ 250°C, 2.0 μL | Oven Program: | 120°C for 1 min to 220°C at 20°C/min for 16 min to 235°C at 5°C/min for 7 min to 300°C at 5°C/min for 15 min | Carrier Gas: | Constant Flow Helium, 26.0 cm/sec | Detection: | High Res Mass Spec (HRMS) (290°C) | Sample Notes: | Notes: Flow 26cm/sec @ 200°C. Only selected chromatograms shown below. For the complete set of Single Ion Chromatograms, showing both Polychlorinated Dibenzo-p-dioxins and Polychlorinated Dibenzofurans, please contact your Phenomenex Technical Consultant.
Mass Chromatograms are courtesy of V.N. Fishman, G.D. Martin, and L.L. Lamparski, The Dow Chemical Company, Midland, Michigan, USA
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3. 2,3,7,8-TCDF / possible unknown TCDF 5. 1,3,4,6,8/1,2,4,6,8-PnCDF 7. 2,3,4,7,8-PnCDF / unknown PnCDF |