| 1Metanephrine |
|---|
| 2Normetanephrine |
Compound Name Metanephrine |
CID 21100 |
Molecular Formula C10H15NO3 |
Molecular Weight 197 |
No. Chiral Centers: 1 |
No. Hydrogen Bond Acceptors 4 |
No. Hydrogen Bond Donors 3 |
Applications
Metanephrine and Normetanephrine on Luna HILIC 3um 50X2.0mm
18291
Clinical
Clinical Research
Therapeutic / Clinical
Analytes
Details
LC Conditions (App ID: 18291)
Elution Type: Gradient | ||||||||||||||||||||||||
Mobile Phase: A: 95/5 ACN/100 mM ammonium formate, pH 3.2 B: 50/45/5 ACN/Water/100 mM ammonium formate, pH 3.2 | ||||||||||||||||||||||||
Gradient Profile:
| ||||||||||||||||||||||||
Flow Rate: 0.4 mL/min | ||||||||||||||||||||||||
Temperature: 22°C | ||||||||||||||||||||||||
Detection: Mass Spectrometer (MS) (22°C) | ||||||||||||||||||||||||
Sample Note: LC/MS/MS & Chromatographic Condition
MS Detector: API 3000 LC/MS/MS with ESI (TurboIonSpray®) (www.Appliedbiosystems.com), Positive Ion Mode; MRM; heater gas flow 7000 cc/min; heater temperature 550 °C; Column: LUNA 3µm HILIC, 50x2.0mm; Flow rate: 0.4ml/min
ESI Source Conditions:
NEB: 9.00
CUR: 10.00
IS: 3500.00
TEM: 550.00
CAD: 11.00
CE 23.00 Normetanephrine
CE 25.00 Metanephrine
Analyte Q1 Q3 Time DP FP CE CXP
NMN 166.4 134.2 150 61 370 23 8
MN 180.4 148.2 150 71 370 25 8 |
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