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Opiates from urine by Strata-XC on a ZB-Drug1

Sample Preparation Details

Part No:8B-S029-TBJ
Solid Phase Extraction (SPE) procedure:Note: The solvent volumes shown below are for a 30 mg bed mass. The solvent volumes will need to be adjusted for a smaller or larger bed mass.
Load:To 1 mL of urine add 0.5 mL of 0.1 N HCl adjust pH to 6.0 using 1% phosphoric acid
Dry:10 min @ >10" Hg
Final Prep and Analysis: Inject: 1 µL on GC / Mass Selective (MSD) @ amu / (320 °C)

Analytes:

Name Spiked
Conc.
Log P pKa % Rec %RSC (n=0)
1 Codeine-d6
2 Codeine
3 Morphine-d3
4 Morphine

Application Detail (App ID: 18301)

Part No:7CD-G023-08
Phase:Proprietary Drug Phase
Dimensions:10 meters x 0.18 mm x 0.18 µm
Oven Profile:185 ºC to 320 ºC @ 30 ºC/min for 3 min
Carrier Gas:Constant Flow Helium, 0.7 mL/min
Injection:Split 10:1 1 µL @ 260°C
Detection: Mass Selective (MSD) (320°C)
Note:Analytes are 300 ng/mL in urine derivatized with propionic anhydride
Sim ions:
(Quant ion*) D6-Codeine (*361,288,235): Codeine (*355,282,229): D3-Morphine (*344,271,400): Morphine (*341,268,397)

Analyte Details

Analyte Detail not available

1
Codeine-d6
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2
Codeine
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3
Morphine-d3
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4
Morphine
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