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Opiates from urine by Strata-XC on a ZB-Drug1

Sample Preparation Details

Condition 1 :1 mL Methanol at 1 mL/min
Condition 2 :1 mL Water at 1 mL/min
Load :Load 1.00 mL Sample diluted in Urine
Wash 1 :1 mL 0.1 N HCl at 1 mL/min
Wash 2 :1 mL Methanol at 1 mL/min
Dry :10 min @ >10" Hg
Elution 1 :1 mL Methanol with 5% ammonium hydroxide at 1 mL/min
Evaporate: :Evaporate to dryness
Reconstitute :50 µL Ethyl acetate

Application Detail (App ID: 18301)

Part No:7CD-G023-08
Phase:Proprietary Drug Phase
Dimensions:10 meters x 0.18 mm x 0.18 µm
Oven Profile:185 ºC to 320 ºC @ 30 ºC/min for 3 min
Carrier Gas:Constant Flow Helium, 0.7 mL/min
Injection:Split 10:1 1 µL @ 260°C
Detection: Mass Selective (MSD) (320°C)
Note:Analytes are 300 ng/mL in urine derivatized with propionic anhydride
Sim ions:
(Quant ion*) D6-Codeine (*361,288,235): Codeine (*355,282,229): D3-Morphine (*344,271,400): Morphine (*341,268,397)

Analyte Details

Analyte Detail not available

1
Codeine-d6
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2
Codeine
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3
Morphine-d3
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4
Morphine
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