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Benzoylecgonine from urine by Strata-XC on a ZB-Drug1

Sample Preparation Details

Condition 1 :1 mL Methanol at 1 mL/min
Condition 2 :1 mL Water at 1 mL/min
Condition 3 :1 at 1
Load :Load 1.00 mL Sample diluted in Urine
Wash 1 :1 mL HCl (0.1N) at 1 mL/min
Wash 2 :1 mL Methanol at 1 mL/min
Wash 3 :3 at 1
Dry :5 minutes at > 10 inch Hg
Elution 1 :1 mL Methanol with 5% NH3OH at 1 mL/min
Evaporate: :Evaporate to dryness
Reconstitute :50 µL BSTFA/Pyridine

Application Detail (App ID: 18416)

Part No:7CD-G023-08
Phase:Proprietary Drug Phase
Dimensions:10 meters x 0.18 mm x 0.18 µm
Oven Profile:235 °C to 320 °C @ 25 °C/min for 1min
Carrier Gas:Constant Flow Helium, 55 cm/sec
Injection:Split 10:1 1 µL @ 260°C
Detection: Mass Selective (MSD) (320°C)
Note:Analytes are 300ng/mL extracted from urine then derivatized with BSTFA
Sim ions:
(Quant ion*) D3-Benzoylecgonine (*85,243,364): Benzoylecgonine (*82,240,361)

Analyte Details

Analyte Detail not available

1
Benzoylecgonine-d3
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2
Benzoylecgonine
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