Region

Applications

Expanded amphetamines from urine by Strata-XC on a ZB-Drug1

Sample Preparation Details

Part No:8B-S029-TBJ
Solid Phase Extraction (SPE) procedure:Note: The solvent volumes shown below are for a 30 mg bed mass. The solvent volumes will need to be adjusted for a smaller or larger bed mass.
Load:Add 1 mL of 100 mM phosphate buffer (pH 6.0) adjust pH to 6.0 using 2% phosphoric acid
Dry:5 minutes at >10 in Hg
Final Prep and Analysis: Inject: 1 µL on GC / Mass Selective (MSD) @ amu / (320 °C)

Analytes:

Name Spiked
Conc.
Log P pKa % Rec %RSC (n=0)
1 Amphetamine-d11
2 Amphetamine
3 Methamphetamine-d14
4 Methamphetamine
5 MDA-d5
6 MDA
7 MDMA-d5
8 MDMA
9 MDEA-d5
10 MDEA

Application Detail (App ID: 18482)

Part No:7CD-G023-08
Phase:Proprietary Drug Phase
Dimensions:10 meters x 0.18 mm x 0.18 µm
Oven Profile:70 °C to 130 °C @ 20 °C/min to 320 °C @ 30 °C/min for 0.67 min
Carrier Gas:Constant Flow Helium, 0.7 mL/min
Injection:Split 10:1 1 µL @ 260°C
Detection: Mass Selective (MSD) (320°C)
Note:Analytes are 500ng/mL in urine derivatized with HFBA
Sim ions:
(Quant ion*) D11-Amphetamine (*244,128): Amphetamine (*240,118,117): D14-Methamphetamine (*261,213): Methamphetamine (*254,210,118): D5-MDA (*167,380,244): MDA (*162,375,240): D5-MDMA (*258,213,164): MDMA (*254,210,389): D5-MDEA (*273,241,408): MDEA (*268,240,403)

Analyte Details

Analyte Detail not available

1
Amphetamine-d11
search

2
Amphetamine
search

3
Methamphetamine-d14
search

4
Methamphetamine
search

5
MDA-d5
search

6
MDA
search

7
MDMA-d5
search

8
MDMA
search

9
MDEA-d5
search

10
MDEA
search