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Expanded amphetamines from urine by Strata-XC on a ZB-Drug1

Sample Preparation Details

Condition 1 :1 mL Methanol at 1 mL/min
Condition 2 :1 mL Water at 1 mL/min
Condition 3 :3 at 1
Load :Load 1.00 mL Sample diluted in Urine
Wash 1 :1 mL 0.1 N HCl at 1 mL/min
Wash 2 :1 mL Methanol at 1 mL/min
Wash 3 :3 at 1
Dry :5 minutes at >10 in Hg
Elution 1 :1 mL 5% Ammonium hydroxide in methanol at 1 mL/min
Evaporate: :Evaporate to dryness
Reconstitute :100 µL initial mobile phase

Application Detail (App ID: 18482)

Part No:7CD-G023-08
Phase:Proprietary Drug Phase
Dimensions:10 meters x 0.18 mm x 0.18 µm
Oven Profile:70 °C to 130 °C @ 20 °C/min to 320 °C @ 30 °C/min for 0.67 min
Carrier Gas:Constant Flow Helium, 0.7 mL/min
Injection:Split 10:1 1 µL @ 260°C
Detection: Mass Selective (MSD) (320°C)
Note:Analytes are 500ng/mL in urine derivatized with HFBA
Sim ions:
(Quant ion*) D11-Amphetamine (*244,128): Amphetamine (*240,118,117): D14-Methamphetamine (*261,213): Methamphetamine (*254,210,118): D5-MDA (*167,380,244): MDA (*162,375,240): D5-MDMA (*258,213,164): MDMA (*254,210,389): D5-MDEA (*273,241,408): MDEA (*268,240,403)

Analyte Details

Analyte Detail not available

1
Amphetamine-d11
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2
Amphetamine
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3
Methamphetamine-d14
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4
Methamphetamine
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5
MDA-d5
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6
MDA
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7
MDMA-d5
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8
MDMA
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9
MDEA-d5
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10
MDEA
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