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Propoxyphene from urine by Strata-XC on a ZB-Drug1

Sample Preparation Details

Condition 1 :1 mL Methanol at 1 mL/min
Condition 2 :1 mL Water at 1 mL/min
Condition 3 :1 at 1
Load :Load 2.00 mL Sample diluted in Urine
Wash 1 :1 mL 0.1 N HCl at 1 mL/min
Wash 2 :1 mL Methanol at 1 mL/min
Wash 3 :3 at 1
Dry :5 minutes at > 10 inch Hg
Elution 1 :1 mL 5% NH3OH in Methanol at 1 mL/min
Evaporate: :Evaporate to dryness
Reconstitute :50 µL Ethyl acetate

Application Detail (App ID: 18486)

Part No:7CD-G023-08
Phase:Proprietary Drug Phase
Dimensions:10 meters x 0.18 mm x 0.18 µm
Oven Profile:200 °C to 320 °C @ 25 °C/min
Carrier Gas:Constant Flow Helium, 55 cm/sec
Injection:Split 20:1 1 µL @ 260°C
Detection: Mass Selective (MSD) (320°C)
Note:Analytes are 300ng/mL in urine
Sim ions:
(Quant ion*) D11-Propoxyphene (*64,198,213): Propoxyphene (*58,193,208)

Analyte Details

Analyte Detail not available

1
Propoxyphene-d11
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2
Propoxyphene
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