Region

Applications

EPA 8330 - High-Speed Screening of Explosives using Kinetex 2.6µm C18 100 x 4.6mm ID

Sample Preparation Details

Part No:8B-S043-HCH
Solid Phase Extraction (SPE) procedure:Note: The solvent volumes shown below are for a 500 mg bed mass. The solvent volumes will need to be adjusted for a smaller or larger bed mass.
Dry:3-5 min at 10 mm Hg
Final Prep and Analysis: Inject: 0.5 µL on HPLC / UV-Vis Abs.-Diode Array (PDA) @ 254 nm (ambient)

Analytes:

Name Spiked
Conc.
Log P pKa % Rec %RSC (n=0)
1 HMX
2 RDX
3 1,3,5-Trinitrobenzene
4 1,3-Dinitrobenzene
5 Tetryl
6 Nitrobenzene
7 2,4,6-Trinitrotoluene
8 2-Amino-4,6-dinitrotoluene
9 4-Amino-2,6-dinitrotoluene
10 2,6-Dinitrotoluene
11 2,4-Dinitrotoluene
12 2-Nitrotoluene
13 4-Nitrotoluene
14 3-Nitrotoluene

Application Detail (App ID: 18556)

Part No:00D-4462-E0
Dimensions:100 x 4.6 mm ID
Elution Type:Gradient
Elution A:Water
Elution B:Methanol
Gradient Profile:
Step No. Time (min) Pct A Pct B
1 0 45 55
2 5 35 65

Flow Rate:1.4 mL/min
Col. Temp: ambient
Detection: UV-Vis Abs.-Diode Array (PDA) @ 254 nm (22°C)
Note:SecurityGuard™ ULTRA Guard Cartridge System extends column lifetime.
- SecurityGuard ULTRA Cartridges, UHPLC C18 for 4.6mm ID Columns, 3/Pk Part No.: AJ0-8768
- Holder Part No.: AJ0-9000

Analyte Details

Analyte Detail not available

1
HMX
search

2
RDX
search

3
1,3,5-Trinitrobenzene
search

4
1,3-Dinitrobenzene
search

5
Tetryl
search

6
Nitrobenzene
search

7
2,4,6-Trinitrotoluene
search

8
2-Amino-4,6-dinitrotoluene
search

9
4-Amino-2,6-dinitrotoluene
search

10
2,6-Dinitrotoluene
search

11
2,4-Dinitrotoluene
search

12
2-Nitrotoluene
search

13
4-Nitrotoluene
search

14
3-Nitrotoluene
search