Region

Applications

Extraction of Carbamate Pesticides using Strata-X on Kinetex 2.6µm C18 50 x 2.1mm ID by LCMS

Sample Preparation Details

Condition 1 :1 mL Methanol at 2 mL/min
Condition 2 :1 mL 25 mM ammonium acetate pH 5.5 at 2 mL/min
Load :Load 0.40 mL Sample diluted in 1
Wash 1 :1 mL 25 mM ammonium acetate pH 5.5 at 2 mL/min
Wash 2 :1 mL 15% methanol at 2 mL/min
Dry :2 mins at 10" of Hg
Elution 1 :0.5 mL 5% formic acid/methanol at 1 mL/min
Elution 2 :0.5 mL 5% formic acid/methanol at 1 mL/min
Evaporate: :Evaporate to dryness
Reconstitute :200 µL 97/3 initial LC mobile phase

Application Detail (App ID: 18638)

Part No:00B-4462-AN
Dimensions:50 x 2.1 mm ID
Elution Type:Gradient
Elution A:5mM Ammonium formate in H2O
Elution B:mM Ammonium formate in ACN
Gradient Profile:
Step No. Time (min) Pct A Pct B
1 0 97 3
2 0.25 97 3
3 2.5 5 95
4 4 5 95
5 4.01 97 3
6 5.5 97 3

Flow Rate:500 µL/min
Col. Temp: 25 °C
Detection: Mass Spectrometer (MS) @ amu (22°C)
Note:SecurityGuard™ ULTRA Guard Cartridge System extends column lifetime.
- SecurityGuard ULTRA Cartridges, UHPLC C18 for 2.1mm ID Columns, 3/Pk Part No.: AJ0-8782
- Holder Part No.: AJ0-9000

Analyte Details

Analyte Detail not available

1
Aldicarb-sulfoxide
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2
Aldicarb-sulfone
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3
Oxamyl
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4
Methomyl
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5
3-Hydroxy carbofuran
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6
Aldicarb
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7
Carbofuran and D3
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8
Methiocarb
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