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Applications

Opiates from urine using Strata-X-Drug B and Zebron Drug-1 10x0.18x0.18

Sample Preparation Details

Load :Load 2.00 mL Sample diluted in Pre-Treated Sample
Wash 1 : 2mL of Sodium Acetate (100mM), pH 5.0
Wash 2 : 2mL of Methanol
Dry :10 min @ 10" Hg
Elution 1 : 2mL of Ethyl Acetate: IPA:NH4OH (7:2:1)
Evaporate: :Evaporate to dryness
Reconstitute :100 µL Ethyl Acetate
Notes :Evaporate eluant to dryness at 50°C. Add 50uL of Propionic anhydride and 50uL of acetonitrile. Heat 30 mins at 60°C. Evaporate to dryness at 50°C. Reconstitute in 100uL of Ethyl Acetate

Application Detail (App ID: 19600)

Part No:7CD-G023-08
Phase:Proprietary Drug Phase
Dimensions:10 meters x 0.18 mm x 0.18 µm
Oven Profile:185°C to 320°C @ 30°C/min. Hold 3.00 mins
Carrier Gas:Constant Flow Helium, 0.7 mL/min
Injection:Split 20:1 1 µL @ 260°C
Detection: Mass Selective (MSD) (320°C)
Note:Analytes are spiked into urine @ SAMSHA cutoff level of 2000ng/mL

Analyte Details

Analyte Detail not available

1
Codeine-d3
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2
Codeine
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3
Morphine-d3
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4
Morphine
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