Region

Applications

Sulfonamides in Meat by LC/MS/MS

Sample Preparation Details

Condition 1 :4 mL Methanol
Condition 2 :4 mL 0.1% Formic Acid in Water
Load :Load 4.00 mL Sample diluted in 0.1% Formic Acid/Methanol (95:5)
Wash 1 :2 mL 0.1% Formic Acid in Water
Dry :2min at 10inches Hg
Elution 1 :1 mL Methanol
Evaporate: :Evaporate to dryness
Reconstitute :250 µL 90:10 water:methanol, containing 0.1% formic acid

Application Detail (App ID: 20036)

Part No:00B-4439-E0
Dimensions:50 x 4.6 mm ID
Elution Type:Gradient
Elution A:0.1% Formic Acid in Water
Elution B:Acetonitrile
Gradient Profile:
Step No. Time (min) Pct A Pct B
1 0 98 2
2 2 98 2
3 2.1 85 15
4 6.5 50 50
5 7.1 0 100
6 8 0 100
7 8.1 98 2
8 10 98 2

Flow Rate:800 µL/min
Col. Temp: ambient
Detection: Tandem Mass Spec (MS-MS) @ (300°C)
Detector Info: AB Sciex 3200 QTRAP®
Note:SecurityGuard™ Guard Cartridge System extends column lifetime.
- SecurityGuard Cartridges, Gemini C18 4 x 3.0mm ID, 10/Pk Part No.: AJ0-7597
- Holder Part No.: KJ0-4282

Analyte Details

Analyte Detail not available

1
Sulfadiazine
search

2
Sulfathiazole
search

3
Sulfapyridine
search

4
Sulfamerazine
search

5
Sulfamethazine
search

6
Sulfamethoxazole
search

7
Sulfadimethoxine
search

8
Sulfaquinoxaline
search