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Mycotoxins extracted from corn using roQ by LC/MS/MS (Positive mode)

Application Detail (App ID: 22711)

Part No:00B-4496-AN
Dimensions:50 x 2.1 mm ID
Elution Type:Gradient
Elution A:5 mM ammonium acetate w/ 0.5% acetic acid
Elution B:5 mM ammonium acetate in methanol w/ 0.5% acetic acid
Gradient Profile:
Step No. Time (min) Pct A Pct B
1 0 95 5
2 2 95 5
3 5 20 80
4 5.2 2 98
5 8 2 98

Flow Rate:0.45 mL/min
Col. Temp: ambient
Detection: Tandem Mass Spec (MS-MS) @ (22°C)
Detector Info: API 5000
Note:roQ extraction:
1) 5 g of corn is extracted using KS0-8909 with 10 mL of water and 10 mL of ACN with 1.0 % formic acid.
2. KSO-8924 is used for dSPE clean up.

Analyte Details

Analyte Detail not available

1
15-Acetyldeoxynivalenol
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2
Aflatoxin G2
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3
Aflatoxin G1
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4
Unknown Interference
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5
Aflatoxin B2
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6
Aflatoxin B1
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7
Diacetoxyscirpenol
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8
HT2-Toxin

9
Fuminosin B1
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10
T2-Toxin
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11
Ochratoxin A
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12
Fuminosin B2