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Carcinogenic amines on Kinetex 2.6 µm EVO C18

Application Detail (App ID: 23042)

Part No:00F-4725-AN
Dimensions:150 x 2.1 mm ID
Elution Type:Gradient
Elution A:10 mM ammonium acetate/ ACN (95:5)
Elution B:Acetonitrile
Gradient Profile:
Step No. Time (min) Pct A Pct B
1 0 95 5
2 10 5 95

Flow Rate:0.4 mL/min
Col. Temp: 50 °C
Detection: UV-Vis Abs.-Variable Wave.(UV) @ 240 nm (22°C)
Note:Forced degradation protocol:
Reconstitute 1 mg of cefaclor neat standard with 1.0 mL of 1 M HCl. Heat the solution at 60 ºC for 6 hours then neutralize with 1.0 mL of 1 M NaOH. Refrigerate until ready to inject.

Analyte Details

Analyte Detail not available

1
4-Methyl-m-phenylenediamine
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2
o-Anisidine
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3
o-Toluidine
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4
Benzidine
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5
4-Chloroaniline
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6
3,3'-Dimethoxybenzidine
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7
3,3'-Dimethylbenzidine
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8
2-Naphthylamine
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9
2,4,5-Trimethylaniline
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10
4,4'-methylenedio-toluidine

11
4-Aminobiphenyl
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12
3,3'-Dichlorobenzidine
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13
2,2'-Dichloro-4,4'-methylenedianiline

14
o-Aminoazotoluene
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