| 1Butalbital-d5 |
|---|
| 2Butalbital |
| 3Amobarbital |
| 4Pentobarbital |
| 5Secobarbital |
| 6Phenobarbital-d5 |
| 7Phenobarbital |
Analyte not found
Applications
Barbiturates from urine by Strata X (60mg/3cc) (TIC)
23895
Separation Mode: Application Specific
Application Specific
ZB-Drug-1
GC
Anticonvulsants
Clinical
Forensics/Toxicology
Analytes
Details
GC Conditions (App ID: 23895)
Column: |
Part No: |
Phase Name: ZB-Drug-1 |
Injection: Split 10:1 @ 280°C, 1.0 μL |
Oven Program: 145 °C to 300 °C @ 25 °C/min |
Carrier Gas: Constant Flow Helium, 0.6 mL/min |
Detection: Mass Selective (MSD) (320°C) |
Sample Notes: Analytes are 300ng/mL in urine derivatized with TMPAH
Sim ions:
(Quant ion*) D5-Butalbital (*201,184,214): Butalbital (*196,181,138): Amobarbital (*169,184,225): Pentobarbital (*169,184,225): Secobarbital (*196,181,138): D5-Phenobarbital (*233,151,122): Phenobarbital (*232,146,117) |
Sample Preparation Details
Description: Strata-X 33 µm Polymeric Reversed Phase, 60 mg / 3 mL, Tubes, 50/Pk |
Part Number: |
Pre Treatment Note: Reconstitute with 100uL Acetonitrile and 50uL of Thermo Scientific MethElute Reagent (TS49301) |
Condition 1: Methanol |
Condition 2: Water |
Condition 3: 20mM potassium phosphate pH 2.7 |
Sample PreTreatment: Reconstitute with 100uL Acetonitrile and 50uL of Thermo Scientific MethElute Reagent (TS49301) |
Wash 1: Water |
Wash 2: 100mM acetic acid |
Evaporation: Evaporate to dryness |
1 Condition Methanol |
2 Wash 100mM acetic acid |
3 Condition 20mM potassium phosphate pH 2.7 |
1 Shake 85:15 Ethyl Acetate:Isopropyl Alcholol |
1 Wash Water |
2 Condition Water |
Order Items Used in This Application
7CD-G023-08
Zebron ZB-Drug-1, GC Cap. Column 10 m x 0.18 mm x 0.18 µm, Ea
Qty:
Similar Applications
search
Butalbital-d5
Kinetex 2.6 µm C18 100 Å, LC Column 100 x 2.1 mm, Ea
Reversed Phase
Zebron ZB-Drug-1, GC Cap. Column 10 m x 0.18 mm x 0.18 µm, Ea
Application Specific
Kinetex 2.6 µm C18 100 Å, LC Column 100 x 2.1 mm, Ea
Reversed Phase
Zebron ZB-Drug-1, GC Cap. Column 10 m x 0.18 mm x 0.18 µm, Ea
Application Specific
Zebron ZB-Drug-1, GC Cap. Column 10 m x 0.18 mm x 0.18 µm, Ea
Application Specific
Zebron ZB-Drug-1, GC Cap. Column 10 m x 0.18 mm x 0.18 µm, Ea
Application Specific
Phenomenex is a technology leader committed to developing novel analytical chemistry solutions that solve the separation and purification challenges of researchers worldwide.
CONNECT WITH US
