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GC/MS analysis of PAH in rubber and plastic on ZB-PAH

Application Detail (App ID: 24508)

Part No:7FD-G038-47
Phase:Proprietary Pesticides Phase
Dimensions:20 meters x 0.18 mm x 0.14 µm
Oven Profile:120°C for 1.0 min to 200°C @ 8°C/min for 0.5 min to 270°C @ 11°C/min to 300°C @ 2°C/min
Carrier Gas:Constant Flow Helium, 52 cm/sec
Injection:Splitless :1 1 µL @ 290°C
Detection: Mass Spectrometer (MS) (250°C)
Note:Sample Preparation:
1. Cut sample of rubber in 2 - 3mm pieces
2. Collect ~0.5g of cut pieces per extraction
3. Add 20mL of toluene
4. Add internal standard
5. Sonicate for 1 hour at 60°C
6. Cool and transfer aliquot to autosampler vial

Analyte Details

Analyte Detail not available

1
Naphthalene-d8
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2
Naphthalene
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3
2-methylnaphtalene

4
1-methylnaphthalene
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5
Acenaphthylene
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6
Acenaphthylene-d10

7
aCENAPHTHENE
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8
Fluorene
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9
Phenanthrene-d10
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10
Phenanthrene
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11
Anthracene
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12
Fluoranthene
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13
Pyrene
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14
p-Terphenyl-d14
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15
Benzo(a)anthracene
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16
Chrysene-d12
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17
Chrysene
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18
Benzo(b)fluoranthene
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19
Benzo(k)fluoranthene
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20
Benzo(j)fluoranthene
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21
Benzo(e)pyrene
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22
Benzo(a)pyrene
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23
Perylene-d12
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24
Indeno(1,2,3-cd)pyrene
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25
Dibenzo(a,h)anthracen

26
Benzo(g,h,i)perylene
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