Applications

EPA Method 8260: Volatile Organics on ZB-624

Analytes

1Dichlorodifluoromethane
2Chloromethane
3Vinyl chloride
4Bromomethane
5Chloroethane
6Trichlorofluoromethane
7Acrolein
81,1,2-Trichloro-1,2,2-trifluorome
91,1-Dichloroethene
10Acetone
11Iodomethane
12Carbon disulfide
13Methyl acetate
14Acetonitrile
15Methylene chloride
16t-Butyl Methyl Ether
17trans-1,2-Dichloroethene
18Acrylonitrile
191,1-Dichloroethane
20Vinyl acetate
212,2 Dichloropropane
222-Butanone
23cis-1,2-Dichloroethene
24Bromochloromethane
25Tetrahydrofuran
26Chloroform
271,1,1-Trichloroethane
28Cyclohexane
29Carbon tetrachloride
301,1-Dichloropropene
311,2-Dichloroethane-d4
32Benzene
331,2-Dichloroethane
341,4-Difluorobenzene
35Trichloroethene
36Methylcyclohexane
371,2-Dichloropropane
38Dibromomethane
39Bromodichloromethane
402-Chloroethyl vinyl ether
41cis-1,3-Dichloropropene
424-Methyl-2-Pentanone
43Toluene-d8
44Toluene
45trans-1,3-Dichloropropene
46Ethyl methacrylate
471,1,2-Trichloroethane
48Tetrachloroethene
491,3-Dichloropropane
502-Hexanone
51Dibromochloromethane
521,2-Dibromoethane
53Chlorobenzene-d5
54Chlorobenzene
55Ethylbenzene
561,1,1,2-Tetrachloroethane
57m/p-Xylene
58o-Xylene
59Styrene
60Bromoform
61Isopropylbenzene
62p-Bromofluorobenzene
631,1,2,2-Tetrachloroethane
64Bromobenzene
65t-1,4-Dichloro-2-Butene
661,2,3-Trichloropropane
67n-Propylbenzene
681,3,5-Trimethylbenzene
692-Chlorotoluene
704-Chlorotoluene
71tert-Butylbenzene
721,2,4-Trimethylbenzene
73sec-Butylbenzene
744-Isopropyltoluene
751,3-Dichlorobenzene
761,4-Dichlorobenzene-d4
771,4-Dichlorobenzene
78n-Butylbenzene
791,2-Dichlorobenzene
801,2-Dibromo-3-Chloropropane
811,2,4-Trichlorobenzene
82Hexachlorobutadiene
83Naphthalene
841,2,3-Trichlorobenzene

Compound Name Halon
CID 6391
Molecular Formula CCl2F2
Molecular Weight 120
No. Hydrogen Bond Acceptors 2

Details

Official Method: EPA 8260

GC Conditions (App ID: 14783)

Column: Zebron ZB-624, GC Cap. Column 60 m x 0.25 mm x 1.40 µm, Ea
Part No: 7KG-G005-27
Phase Name: ZB-624
Injection: Purge and Trap 30:1 @ 250°C, 1.0 μL
Oven Program: 40°C for 2 min to 225°C at 10°C/min for 3.5 min
Carrier Gas: Constant Flow Helium, 1.1 mL/min
Detection: Mass Selective (MSD) (180°C)
Sample Notes: The sample was introduced via a Tekmar 2000 Purge and Trap with the following settings. Purge time was 11.0 minutes with a dry purge time of 2.0 minutes. Desorb preheat was 245ºC and desorb conditions for 2.0 minutes at 250ºC. A bake time of 8.0 minutes was used at 260ºC with valve and lines at 120ºC and a mount at 40ºC.

Order Items Used in This Application

7KG-G005-27

Zebron ZB-624, GC Cap. Column 60 m x 0.25 mm x 1.40 µm, Ea

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Zebron ZB-624, GC Cap. Column 20 m x 0.18 mm x 1.00 µm, Ea

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Zebron ZB-624, GC Cap. Column 60 m x 0.53 mm x 3.00 µm, Ea

Standard

EPA Method 8260: Volatile Organics on ZB-624

Order Items Used in This Application

7KG-G005-27

Zebron ZB-624, GC Cap. Column 60 m x 0.25 mm x 1.40 µm, Ea

Details

GC Conditions

Official Method:	EPA 8260
Column:	Zebron ZB-624, GC Cap. Column 60 m x 0.25 mm x 1.40 µm, Ea
Part No:	7KG-G005-27
	Phase Name:	ZB-624
Injection:	Purge and Trap 30:1 @ 250°C, 1.0 μL
Oven Program:	40°C for 2 min to 225°C at 10°C/min for 3.5 min
Carrier Gas:	Constant Flow Helium, 1.1 mL/min
Detection:	Mass Selective (MSD) (180°C)
Sample Notes:	The sample was introduced via a Tekmar 2000 Purge and Trap with the following settings. Purge time was 11.0 minutes with a dry purge time of 2.0 minutes. Desorb preheat was 245ºC and desorb conditions for 2.0 minutes at 250ºC. A bake time of 8.0 minutes was used at 260ºC with valve and lines at 120ºC and a mount at 40ºC.

Analytes

1. Dichlorodifluoromethane

2. Chloromethane

3. Vinyl chloride

4. Bromomethane

5. Chloroethane

6. Trichlorofluoromethane

7. Acrolein

8. 1,1,2-Trichloro-1,2,2-trifluorome

9. 1,1-Dichloroethene

10. Acetone

11. Iodomethane

12. Carbon disulfide

13. Methyl acetate

14. Acetonitrile

15. Methylene chloride

16. t-Butyl Methyl Ether

17. trans-1,2-Dichloroethene

18. Acrylonitrile

19. 1,1-Dichloroethane

20. Vinyl acetate

21. 2,2 Dichloropropane

22. 2-Butanone

23. cis-1,2-Dichloroethene

24. Bromochloromethane

25. Tetrahydrofuran

26. Chloroform

27. 1,1,1-Trichloroethane

28. Cyclohexane

29. Carbon tetrachloride

30. 1,1-Dichloropropene

31. 1,2-Dichloroethane-d4

32. Benzene

33. 1,2-Dichloroethane

34. 1,4-Difluorobenzene

35. Trichloroethene

36. Methylcyclohexane

37. 1,2-Dichloropropane

38. Dibromomethane

39. Bromodichloromethane

40. 2-Chloroethyl vinyl ether

41. cis-1,3-Dichloropropene

42. 4-Methyl-2-Pentanone

43. Toluene-d8

44. Toluene

45. trans-1,3-Dichloropropene

46. Ethyl methacrylate

47. 1,1,2-Trichloroethane

48. Tetrachloroethene

49. 1,3-Dichloropropane

50. 2-Hexanone

51. Dibromochloromethane

52. 1,2-Dibromoethane

53. Chlorobenzene-d5

54. Chlorobenzene

55. Ethylbenzene

56. 1,1,1,2-Tetrachloroethane

57. m/p-Xylene

58. o-Xylene

59. Styrene

60. Bromoform

61. Isopropylbenzene

62. p-Bromofluorobenzene

63. 1,1,2,2-Tetrachloroethane

64. Bromobenzene

65. t-1,4-Dichloro-2-Butene

66. 1,2,3-Trichloropropane

67. n-Propylbenzene

68. 1,3,5-Trimethylbenzene

69. 2-Chlorotoluene

70. 4-Chlorotoluene

71. tert-Butylbenzene

72. 1,2,4-Trimethylbenzene

73. sec-Butylbenzene

74. 4-Isopropyltoluene

75. 1,3-Dichlorobenzene

76. 1,4-Dichlorobenzene-d4

77. 1,4-Dichlorobenzene

78. n-Butylbenzene

79. 1,2-Dichlorobenzene

80. 1,2-Dibromo-3-Chloropropane

81. 1,2,4-Trichlorobenzene

82. Hexachlorobutadiene

83. Naphthalene

84. 1,2,3-Trichlorobenzene

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