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Applications
ASTM D6584: Free and Total Glycerin in B-100 Biodiesel Methyl Esters
16211
Separation Mode: High Temperature
High Temperature
ASTM D 6584
ZB-5HT
GC
Cryoprotective Agents
Fuels
Alternative Fuel
Energy / Petroleum / Plastic

Applications

ASTM D6584: Free and Total Glycerin in B-100 Biodiesel Methyl Esters
Analytes
1Glycerol
2Butanetriol
3Ester
4Monoglycerides
51-Monooleoyl-rac-glycerol
6Tricaprin
7Diglycerides
81,3-Diolein
9Triglycerides
10Triolein
Compound Name
Glycerol
CID
753
Molecular Formula
C3H8O3
Molecular Weight
92
No. Hydrogen Bond Acceptors
3
No. Hydrogen Bond Donors
3
Details
Official Method: ASTM D 6584
GC Conditions (App ID: 16211)
Column:
Part No:
Phase Name:
ZB-5HT
Injection:
On-Column @ 53°C, 1.0 μL
Oven Program:
50 °C for 1 min. to 180 °C at 15 °C/min. to 230 °C at 7 °C/min. to 380 °C at 30 °C/min. for 10 min.
Carrier Gas:
Constant Flow Helium, 3.0 mL/min
Detection:
Flame Ionization (FID) (380°C)
Sample Notes:
A 2.0 m x 0.53 mm Guard Column was connected to the analytical column per ASTM method requirements.

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