| 1Propoxyphene-d11 |
|---|
| 2Propoxyphene |
Compound Name Levopropoxyphene |
CID 15330 |
Molecular Formula C22H29NO2 |
Molecular Weight 339 |
No. Chiral Centers: 2 |
No. Hydrogen Bond Acceptors 3 |
Applications
LC/MS/MS Analysis of Propoxyphene from urine using Strata-X-Drug B on a Kinetex C18 2.6µm, 50x2.1mm
19704
Separation Mode: Reversed Phase
Reversed Phase
C18
HPLC
Analgesics, Opioid
Forensics/Toxicology
Applications
LC/MS/MS Analysis of Propoxyphene from urine using Strata-X-Drug B on a Kinetex C18 2.6µm, 50x2.1mm
Analytes
Details
LC Conditions (App ID: 19704)
Column: | ||||||||||||||||||||
Brand Name: Kinetex | ||||||||||||||||||||
Part No: | ||||||||||||||||||||
Phase Name: C18 | ||||||||||||||||||||
Elution Type: Gradient | ||||||||||||||||||||
Mobile Phase: A: 0.1% Formic acid B: 0.1% Formic acid in acetonitrile | ||||||||||||||||||||
Gradient Profile:
| ||||||||||||||||||||
Flow Rate: 400 µL/min | ||||||||||||||||||||
Temperature: 0°C | ||||||||||||||||||||
Detection: Mass Spectrometer (MS) (22°C) | ||||||||||||||||||||
Detector Info: SCIEX API 3000™
Source: Cur-11, CAD-12, IS-4500, Tem-450, NEB-12
Dwell: 25ms
Polarity: Positive |
Sample Preparation Details
Description: Strata-X-Drug B 33 µm Polymeric Strong Cation, 60 mg / 6 mL, Tubes, 30/Pk |
Part Number: |
Pre Treatment Note: Evaporate to dryness under a stream of nitrogen at 50 C . Reconstitute in 1 mL of 40% acetonitrile. |
Sample PreTreatment: Evaporate to dryness under a stream of nitrogen at 50 C . Reconstitute in 1 mL of 40% acetonitrile. |
Wash 1: 2 mLs of 100mM Sodium acetate (pH 5.0) buffer |
Wash 2: 2 mLs of Methanol |
Evaporation: Evaporate to dryness |
1 Shake 2mLs of Ethyl acetate:Isopropanol:NH4OH (7:2:1) |
1 Wash 2 mLs of 100mM Sodium acetate (pH 5.0) buffer |
2 Wash 2 mLs of Methanol |
Order Items Used in This Application
00B-4462-AN
Kinetex 2.6 µm C18 100 Å, LC Column 50 x 2.1 mm, Ea
Qty:
Similar Applications
search
Propoxyphene-d11
Zebron ZB-Drug-1, GC Cap. Column 10 m x 0.18 mm x 0.18 µm, Ea
Application Specific
Zebron ZB-Drug-1, GC Cap. Column 10 m x 0.18 mm x 0.18 µm, Ea
Application Specific
Zebron ZB-Drug-1, GC Cap. Column 10 m x 0.18 mm x 0.18 µm, Ea
Application Specific
Phenomenex is a technology leader committed to developing novel analytical chemistry solutions that solve the separation and purification challenges of researchers worldwide.
CONNECT WITH US
