| 1Oxymorphone-d3 |
|---|
| 2Oxymorphone |
| 3Morphine-d3 |
| 4Morphine |
| 5Hydromorphone-d6 |
| 6O-Desmethyltramadol |
| 7Hydromorphone |
| 8Oxycodone-d6 |
| 9Oxycodone |
| 10Codeine-d6 |
| 11Codeine |
| 12N-Desmethyltramadol |
| 13cis-Tramadol |
| 14Hydrocodone-d6 |
| 15Hydrocodone |
| 16Normeperidine-d4 |
| 17Normeperidine |
| 18Meperidine-d4 |
| 19Meperidine |
Compound Name Oxymorphone |
CID 5284604 |
Molecular Formula C17H19NO4 |
Molecular Weight 301 |
No. Hydrogen Bond Acceptors 5 |
No. Hydrogen Bond Donors 2 |
Column: | ||||||||||||||||||||||||
Brand Name: Kinetex | ||||||||||||||||||||||||
Part No: | ||||||||||||||||||||||||
Phase Name: C18 | ||||||||||||||||||||||||
Elution Type: Gradient | ||||||||||||||||||||||||
Mobile Phase: A: 5mM Ammonium acetate B: 5mM Ammonium acetate in methanol | ||||||||||||||||||||||||
Gradient Profile:
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Flow Rate: 500 µL/min | ||||||||||||||||||||||||
Temperature: 0°C | ||||||||||||||||||||||||
Detection: Mass Spectrometer (MS) (22°C) | ||||||||||||||||||||||||
Detector Info: SCIEX API 4000™
Source: Cur-25, CAD-7, IS-5500, Tem-600, GS1 60, GS2 55
Dwell: 20ms
Polarity: Positive
API 4000 |
Description: Strata-X-Drug B 33 µm Polymeric Strong Cation, 60 mg / 6 mL, Tubes, 30/Pk |
Part Number: |
Pre Treatment Note: Evaporate to dryness under a stream of nitrogen at 50 C . Reconstitute in 1 mL of 15% methanol. |
Sample PreTreatment: Evaporate to dryness under a stream of nitrogen at 50 C . Reconstitute in 1 mL of 15% methanol. |
Wash 1: 2mLs of 100mM Sodium acetate (pH 5.0) buffer |
Wash 2: 2mLs of Methanol |
Evaporation: Evaporate to dryness |
1 Shake 2mLs of Ethyl acetate:Isopropanol:NH4OH (7:2:1) |
1 Wash 2mLs of 100mM Sodium acetate (pH 5.0) buffer |
2 Wash 2mLs of Methanol |
