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SPE Method Development Form*
SPE Method Development/Optimization Request
Please fill out this form to the best of your knowledge.
For method development, fill out Part 1
For method optimization, fill out Part 1 &
Part 2
For troubleshooting, fill out Part 1,
Part 2
, &
Part 3
Part 1-Development
Analyte Details
Please list your analyte(s) of interest and concentration. If you do not wish to reveal the exact names, describe analyte(s) in terms of functional groups. (i.e. pKa’s; functional groups; aromaticity; basic; acidic; or neutral ; pH restriction; molecular weight; etc)
Analyte 1
Analyte 2
Analyte 3
Sample Matrix Details
Please describe your sample
Matrix (type)
Volume (mL)
pH
LLOD
LLOQ
Analyte Concentration
Possible Contaminants
Is salt present?
yes
no
Solubility
Aqueous
Organic
Method of Analysis (HPLC, GC or Other)
Notes/Comments
Part 2- Optimization
Please tell us what you would like to improve about your current sample preparation method
Reduced Elution Volumes
Better Reproducibility
Cleaner Extracts
Optimized Recovery
Increased Throughput
Other
Current Recovery %
Ideal Recovery %
Current RSD%
Ideal RSD%
Part 3: Troubleshooting
Please list comments/concerns (e.g. extremely low recovery, clogging, irreproducibility, poor flow )
* = required field
*Salutation
Mr.
Mrs.
Ms.
Dr.
Prof.
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Phamaceutical/BioPharmaceutical/Therapeutics
Life Science/Research Product Supplier
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*Department
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Analysis Laboratory -R&D
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Manufacturing Purification
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Address:
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