| 1Diazepam |
|---|
| 2Nordiazepam-d5 |
| 3Nordiazepam |
| 4Oxazepam-d5 |
| 5Oxazepam |
| 6Temazepam-d5 |
| 7Temazepam |
| 8Clonazepam |
| 9Lorazepam |
| 10Alprazolam |
| 11alpha-Hydroxyalprazolam-d5 |
| 12alpha-Hydroxyalprazolam |
Compound Name Diazepam |
CID 3016 |
Molecular Formula C16H13ClN2O |
Molecular Weight 284 |
No. Hydrogen Bond Acceptors 2 |
Column: |
Part No: |
Phase Name: ZB-Drug-1 |
Injection: Split 10:1 @ 260°C, 1.0 μL |
Oven Program: 200 °C to 210 °C @ 20 °C/min to 320 ºC @ 30ºC/min for 1 min |
Carrier Gas: Constant Flow Helium, 0.7 mL/min |
Detection: Mass Selective (MSD) (320°C) |
Sample Notes: Analytes are 12µg/mL derivatized with MTBSTFA
Sim ions:
(Quant ion*) D5-Nordiazepam (*332,334): Nordiazepam (*327,328,383): D5-Oxazepam (*462,519): Oxazepam (*457,513,459): D5-Temazepam (*362,288,390): Temazepam (*357,359,385): Lorazepam (*491,513,493): Clonazepam (*372,374,326):Diazepam (*256,283,221): Alprazolam (*279,308,204): D5-a-Hydroxyalprazolam (*386,388): a-Hydroxyalprazolam (*381,383,384) |
