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Applications
ASTM D6584: Free and Total Glycerin in B-99.9 Biodiesel Methyl Esters on ZB-XLB-HT
18158
Separation Mode: High Temperature
High Temperature
ASTM D 6584
ZB-XLB-HT
GC
Fuels

Applications

ASTM D6584: Free and Total Glycerin in B-99.9 Biodiesel Methyl Esters on ZB-XLB-HT
Analytes
1Butanetriol
2Esters
3Monoglycerides
41-Monooleoyl-rac-glycerol
5Tricaprin
6Diglycerides
71,3-Diolein
8Triglycerides
9Triolein
Compound Name
2-Deoxyerythritol
CID
18302
Molecular Formula
C4H10O3
Molecular Weight
106
No. Chiral Centers:
1
No. Hydrogen Bond Acceptors
3
No. Hydrogen Bond Donors
3
Details
Official Method: ASTM D 6584
GC Conditions (App ID: 18158)
Column:
Part No:
Phase Name:
ZB-XLB-HT
Injection:
On-Column @ 53°C, 0.1 μL
Oven Program:
50 °C for 1 min to 180 °C @ 15 °C/min to 230 °C @ 7 °C/min to 380 °C @ 30 °C/min for 10 min
Carrier Gas:
Constant Flow Helium, 1.3 mL/min
Detection:
Flame Ionization (FID) (380°C)
Sample Notes:
A 30 cm x 0.53 mm i.d. Guard Column was connected to the analytical column per ASTM method requirements.

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