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Applications
Quantification of Carbamates Fungicides in Beverage by LC/MS/MS
20025
Separation Mode: Reversed Phase
Reversed Phase
C18
HPLC
Molluscacides
Food & Beverage
Product / Trade Good
Product / Trade Good
Environmental / Health
Therapeutic / Clinical
Environmental / Health

Applications

Quantification of Carbamates Fungicides in Beverage by LC/MS/MS
Analytes
1Aldicarb-sulfone
2Methomyl
33-Hydroxycarbofuran
4Oxamyl
5Aldicarb
6Carbofuran
7Carbofuran-d3
8Methiocarb
Compound Name
Aldoxycarb
CID
9570093
Molecular Formula
C7H14N2O4S
Molecular Weight
222
No. Hydrogen Bond Acceptors
5
No. Hydrogen Bond Donors
1
Details
LC Conditions (App ID: 20025)
Column:
Brand Name:
Part No:
Phase Name:
C18
Elution Type:
Gradient
Mobile Phase:
A: 5mM ammonium formate
B: 5mM ammonium formate in acetonitrile
Gradient Profile:
Step No.Time(min)%A%B
108515
22.5595
34595
44.018515
588515
Flow Rate:
0.5 mL/min
Temperature:
28°C
Detection:
Tandem Mass Spec (MS-MS) (22°C)
Detector Info:
3200 QTRAP
Sample Note:
SecurityGuard™ Guard Cartridge System extends column lifetime. - SecurityGuard Cartridges, Gemini C18 4 x 2.0mm ID, 10/Pk Part No.: AJ0-7596 - Holder Part No.: KJ0-4282
Sample Preparation Details
Description:
Strata-X 33 µm Polymeric Reversed Phase, 30 mg / 3 mL, Tubes, 50/Pk
Part Number:
Condition 1:
Methanol
Condition 2:
25mM ammonium acetete pH 5.5
Condition 3:
25mM ammonium acetete pH 5.5
Wash 1:
25mM ammonium acetete pH 5.5
Wash 2:
15% Methanol
Evaporation:
Evaporate to dryness
1
Condition
Methanol
2
Condition
25mM ammonium acetete pH 5.5
3
Condition
25mM ammonium acetete pH 5.5
1
Shake
5% formic acid in methanol
1
Condition
Methanol
2
Condition
25mM ammonium acetete pH 5.5

Order Items Used in This Application

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