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Applications
Food - Quantification of the masked mycotoxin DON-3-glucoside in cereal-based foods by LC/MS/MS
20927
Separation Mode: Reversed Phase
Reversed Phase
C18
HPLC

Applications

Food - Quantification of the masked mycotoxin DON-3-glucoside in cereal-based foods by LC/MS/MS
Analytes
1Deoxynivalenol
2Deoxynivalenol-3-O-glucoside
Compound Name
Vomitoxin
CID
40024
Molecular Formula
C15H20O6
Molecular Weight
296
No. Hydrogen Bond Acceptors
6
No. Hydrogen Bond Donors
3
Details
LC Conditions (App ID: 20927)
Column:
Brand Name:
Kinetex
Part No:
Phase Name:
C18
Elution Type:
Gradient
Mobile Phase:
A: Water with 0.5% Acetic acid
B: Methanol with 0.5% Acetic acid
Gradient Profile:
Step No.Time(min)%A%B
109010
239010
3216040
4274060
5309010
6359010
Flow Rate:
200 µL/min
Temperature:
30°C
System:
Thermo Scient Linear Ion trap LXQ
Detection:
Tandem Mass Spec (MS-MS) (300°C)
Detector Info:
Thermo Scientific linear ion trap LXQ
Sample Note:
Michele Suman E-mail address: michele.suman@barilla.com Barilla Food Research Labs, via Mantova 166, 43100 Parma, Italy

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