| 1C11:0 |
|---|
| 2C16:0 |
| 3C18:0 |
| 4C18:1 cis 9 |
| 5C18:2 cis 9,12 |
| 6C18:3 cis 9,12,15 |
| 7C20:0 |
| 8C20:1 cis 11 |
| 9C22:0 |
Compound Name Methyl Undecanoate |
CID 15607 |
Molecular Formula C12H24O2 |
Molecular Weight 200 |
No. Hydrogen Bond Acceptors 2 |
Applications
FAMEs In Soybean Oil by GC/FID on Zebron ZB-FAME (30 m)
23860
Separation Mode: Application Specific
Application Specific
ZB-FAME
GC
Enzyme Inhibitors
Food & Beverage
Analytes
Details
GC Conditions (App ID: 23860)
Column: |
Part No: |
Phase Name: ZB-FAME |
Injection: Split 50:1 @ 240°C, 1.0 μL |
Oven Program: 100 °C for 2 min to 140 °C @ 10 °C/min to 190 °C @ 3 °C/min to 260 °C @ 30 °C/min for 2 min |
Carrier Gas: Constant Flow Helium, 1.2 mL/min |
Detection: Flame Ionization (FID) (260°C) |
Sample Notes: Recommended Liner: Zebron PLUS Single Taper with Wool, 4 mm ID
Liner Part No.: AG2-0A11-05 (for Agilent systems)
Inlet Seal: AG0-8620 (Gold Plated Easy Seal)
Septum: AG0-4696 (PhenoRed-400)
Sample Preparation:
1. Strata® Si-1 Tube, 1 g/6 mL (Part No.: 8B-S012-JCH) on a vacuum or positive pressure manifold
2. Wash cartridge with 6 mL of hexane
3. Load oil solution (0.12 g of oil in 0.5 mL of hexane)
4. Elute with 10 mL of hexane/diethyl ether (87:13)
5. Evaporate eluate under a steady stream of nitrogen
6. Dissolve purified oil residue in 1mL of heptane
7. Add 0.1 mL of 2N potassium hydroxide in methanol to purified oil solution
8. Cap tube and shake vigorously for 15 seconds
9. Leave to separate until upper layer becomes clear
10. Extract upper layer for GC analysis |
Sample Preparation Details
Description: Strata SI-1 Silica (55 µm, 70 Å), 1 g / 6 mL, Tubes, 30/Pk |
Part Number: |
Pre Treatment Note: To reconstituted sample, add 0.1 mL of 2 N Potassium hydroxide in methanol. Cap tube and shake vigorously for 15 seconds. Leave to separate until upper layer becomes clear. Extract upper layer for GC anlaysis. |
Condition 1: Hexane |
Sample PreTreatment: To reconstituted sample, add 0.1 mL of 2 N Potassium hydroxide in methanol. Cap tube and shake vigorously for 15 seconds. Leave to separate until upper layer becomes clear. Extract upper layer for GC anlaysis. |
Evaporation: Evaporate to dryness |
1 Condition Hexane |
1 Shake Hexane/Diethyl ether (87:13) |
Order Items Used in This Application
7HG-G033-10
Zebron ZB-FAME, GC Cap. Column 30m x 0.25mm x 0.2 µm, Ea
Qty:
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C11:0
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