Diazpam Analysis in Urine
LC Conditions
Column
Onyx Monolithic C18, LC Column 100 x 4.6 mm, Ea
Brand
Onyx
Part No
CH0-7643
Phase Name
Monolithic C18
Elution Type
Gradient
Mobile Phase
A: 0.1% formic acid in Water
B: 0.1% formic acid in Acetonitrile
Gradient Profile
Step No.
Time(min)
%A
%B
1
0
95
5
2
4
10
90
Flow Rate
4.00 mL/min
Temperature
30°C
Detection
Mass Spectrometer (MS) @ (22°C)
Detection Info
Order Items Used in This Application
- 1. Nordiazepam
- 2. Diazepam
-OEChem-06211003152D<br><br> 30 32 0 0 0 0 0 0 0999 V2000<br> 7.0444 -0.1360 0.0000 Cl 0 0 0 0 0 0 0 0 0 0 0 0<br> 2.0000 -2.8430 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0<br> 3.5984 -2.2836 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0<br> 2.6235 -0.2592 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0<br> 4.3802 -0.6602 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 3.5984 -0.0367 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 4.3802 -1.6602 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 3.8209 0.9383 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 5.2742 -0.1255 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 2.1896 -1.1602 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 5.2742 -2.1948 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 2.6235 -2.0611 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 6.1803 -0.6393 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 6.1803 -1.6810 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 4.7765 1.2330 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 3.0879 1.6184 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 4.9990 2.2079 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 3.3104 2.5934 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 4.2660 2.8881 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 5.2670 0.4945 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 3.7364 -2.8881 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 1.7049 -0.7736 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 1.7049 -1.5467 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 5.2670 -2.8148 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 6.7160 -1.9930 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 5.2310 0.8113 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 2.4954 1.4357 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 5.5915 2.3907 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 2.8559 3.0151 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 4.4039 3.4926 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 1 13 1 0 0 0 0<br> 2 12 2 0 0 0 0<br> 3 7 1 0 0 0 0<br> 3 12 1 0 0 0 0<br> 3 21 1 0 0 0 0<br> 4 6 2 0 0 0 0<br> 4 10 1 0 0 0 0<br> 5 6 1 0 0 0 0<br> 5 7 2 0 0 0 0<br> 5 9 1 0 0 0 0<br> 6 8 1 0 0 0 0<br> 7 11 1 0 0 0 0<br> 8 15 2 0 0 0 0<br> 8 16 1 0 0 0 0<br> 9 13 2 0 0 0 0<br> 9 20 1 0 0 0 0<br> 10 12 1 0 0 0 0<br> 10 22 1 0 0 0 0<br> 10 23 1 0 0 0 0<br> 11 14 2 0 0 0 0<br> 11 24 1 0 0 0 0<br> 13 14 1 0 0 0 0<br> 14 25 1 0 0 0 0<br> 15 17 1 0 0 0 0<br> 15 26 1 0 0 0 0<br> 16 18 2 0 0 0 0<br> 16 27 1 0 0 0 0<br> 17 19 2 0 0 0 0<br> 17 28 1 0 0 0 0<br> 18 19 1 0 0 0 0<br> 18 29 1 0 0 0 0<br> 19 30 1 0 0 0 0<br>M END
Compound Name
Nordiazepam
CID
2997
Molecular Formula
C15H11ClN2O
Molecular Weight
270
No. Hydrogen Bond Acceptors
2
No. Hydrogen Bond Donors
1
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