TMS Sugars on ZB-MR1

GC Conditions

Column

Zebron ZB-MultiResidue-1, GC Cap. Column 30 m x 0.25 mm x 0.25 µm, Ea

Part No

7HG-G016-11

Phase Name

ZB-MultiResidue-1

Injection

Split 100:1 @ 225°C

Carrier Gas

Constant Flow Helium, 2.0 mL/min

Detection

Flame Ionization (FID) @ (250°C)

Detection Info

Sample Notes

Sugar mix concentration 176 ppm. Sample was blown dry and then reconstituted in 100uL of 1:1 pyridine/BSTFA+1%TCMS, then heated at 70 °C for 20 minutes, cooled to room temperature, then injected.