Glycols and Benzene in Toothpaste by FID on ZB-WAXplus
GC Conditions
Column
Zebron ZB-WAXplus, GC Cap. Column 30 m x 0.25 mm x 0.25 µm, Ea
Part No
7HG-G013-11
Phase Name
ZB-WAXplus
Injection
Split 20:1 @ 225°C
Carrier Gas
Constant Flow Helium, 3.0 mL/min
Detection
Flame Ionization (FID) @ (250°C)
Detection Info
Sample Notes
0.1 mg toothpaste in 1 ml 50:50 acetonitrile/H2O. 100 ul supernatant to 400 ul acetonitrile/water solvent. To 250 ul sample prep add 25 ul 5 mg/ml 1,3-propanediol (istd).
Order Items Used in This Application
- 1. Acetonitrile
- 2. 1,2-Propanediol
- 3. Ethylene glycol (EG)
- 4. 1,3-Propanediol
- 5. Glycerol
-OEChem-06211003152D<br><br> 6 5 0 0 0 0 0 0 0999 V2000<br> 3.7320 0.5000 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0<br> 2.0000 -0.5000 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 2.8660 0.0000 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 1.6900 0.0369 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 1.4631 -0.8100 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 2.3100 -1.0369 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 1 3 3 0 0 0 0<br> 2 3 1 0 0 0 0<br> 2 4 1 0 0 0 0<br> 2 5 1 0 0 0 0<br> 2 6 1 0 0 0 0<br>M END
Compound Name
Acetonitrile
CID
6342
Molecular Formula
C2H3N
Molecular Weight
41
No. Hydrogen Bond Acceptors
1
Similar Applications
Improved Performance
Glycols and Benzene in Toothpaste Standard on ZB-WAXplus
Zebron ZB-WAXplus, GC Cap. Column 30 m x 0.25 mm x 0.25 µm, Ea
16510
Improved Performance
Glycols and Benzene in Toothpaste by FID on ZB-WAXplus
Zebron ZB-WAXplus, GC Cap. Column 30 m x 0.25 mm x 0.25 µm, Ea
16420