Organotins by MSD on a ZB-5MS
GC Conditions
Column
Zebron ZB-5MS, GC Cap. Column 30 m x 0.25 mm x 0.25 µm, Ea
Part No
7HG-G010-11
Phase Name
ZB-5MS
Injection
Splitless 20:1 @ 240°C
Carrier Gas
Constant Flow Helium, 1.3 mL/min
Detection
Mass Selective (MSD) @ (230°C)
Detection Info
Sample Notes
MSD: sim mode 121,179,235 m/z The analytes are 10ppm, simultaneous L:L extraction and derivatization using Sodium Tetraethylborate.
Order Items Used in This Application
- 1. Monobutyltin
- 2. Tripropyltin
- 3. Dibutyltin
- 4. Tributyltin
- 5. Tetrabutyltin
-OEChem-05151001052D<br><br> 14 13 0 0 0 0 0 0 0999 V2000<br> 5.4641 -0.2500 0.0000 Sn 0 1 0 0 0 0 0 0 0 0 0 0<br> 3.7320 -0.2500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 2.8660 0.2500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 4.5981 0.2500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 2.0000 -0.2500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 3.3335 -0.7249 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 4.1306 -0.7249 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 3.2646 0.7249 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 2.4675 0.7249 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 4.9966 0.7249 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 4.1996 0.7249 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 1.6900 0.2869 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 1.4631 -0.5600 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 2.3100 -0.7869 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 1 4 1 0 0 0 0<br> 2 3 1 0 0 0 0<br> 2 4 1 0 0 0 0<br> 2 6 1 0 0 0 0<br> 2 7 1 0 0 0 0<br> 3 5 1 0 0 0 0<br> 3 8 1 0 0 0 0<br> 3 9 1 0 0 0 0<br> 4 10 1 0 0 0 0<br> 4 11 1 0 0 0 0<br> 5 12 1 0 0 0 0<br> 5 13 1 0 0 0 0<br> 5 14 1 0 0 0 0<br>M CHG 1 1 3<br>M END
Compound Name
Monobutyltin
CID
54267
Molecular Formula
C4H9Sn+3
Molecular Weight
175
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