6-MAM and Interferences by MSD on a ZB-Drug1

GC Conditions

Column

Zebron ZB-Drug-1, GC Cap. Column 10 m x 0.18 mm x 0.18 µm, Ea

Part No

7CD-G023-08

Phase Name

ZB-Drug-1

Injection

Split 10:1 @ 260°C

Carrier Gas

Constant Flow Helium, 0.7 mL/min

Detection

Mass Selective (MSD) @ (320°C)

Detection Info

Sample Notes

Analytes are 24ppm derivatized with BSTFA. Note, Hydromorphone has multiple peaks due to isomers formed during derivatization. Sim ions: (Quant ion*) D3-6-MAM (*402,403): 6-MAM (*399,400,340)