Food - Quantitative Analysis of Glyphosate, Glufosinate and AMPA by LC/MS/MS (FMOC derivatization)

LC Conditions

Column

Gemini 3 µm C18 110 Å, LC Column 150 x 2 mm, Ea

Brand

Gemini

Part No

00F-4439-B0

Phase Name

C18

Elution Type

Gradient

Mobile Phase

A: Water + 2mM Ammonium Carbonate Buffer (pH=9)

B: Methanol

Gradient Profile

Step No.

Time(min)

%A

%B

1

0

99

1

3

4

99

1

4

10

37

63

5

11

37

63

6

25

5

95

Flow Rate

350.00 mL/min

Temperature

30°C

Detection

Mass Spectrometer (MS) @ (300°C)

Detection Info

Sample Notes

SecurityGuard™ Guard Cartridge System extends column lifetime. - SecurityGuard Cartridges, Gemini C18 4 x 2.0mm, 10/Pk Part No.: AJ0-7596 - Holder Part No.: KJ0-4282