b-Blockers (Bupranolol) on Lux 5 µm Cellulose-1 by Chiral SFC
LC Conditions
Column
Lux 5 µm Cellulose-1, LC Column 250 x 4.6 mm, Ea
Brand
Lux
Part No
00G-4459-E0
Phase Name
Cellulose-1
Elution Type
Isocratic
Mobile Phase
A: Methanol with 0.1% DEA
B: Carbon Dioxide
Gradient Profile
Step No.
Time(min)
%A
%B
1
0
20
80
Flow Rate
1.00 mL/min
Temperature
35°C
Detection
UV-Vis Abs.-Diode Array (PDA) @ (22°C)
Detection Info
Sample Notes
Application using Jasco SFC instrument courtesy of Cephalon, Inc.
Order Items Used in This Application
- 1. Bupranolol
- 2. Bupranolol
-OEChem-06211003142D<br><br> 40 40 0 1 0 0 0 0 0999 V2000<br> 2.0000 -1.6830 0.0000 Cl 0 0 0 0 0 0 0 0 0 0 0 0<br> 3.7320 1.3170 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0<br> 3.7320 -0.6830 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0<br> 5.4641 2.3170 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0<br> 6.3301 2.8170 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 5.4641 1.3170 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 4.5981 0.8170 0.0000 C 0 0 3 0 0 0 0 0 0 0 0 0<br> 7.1962 3.3170 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 5.8301 3.6830 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 6.8301 1.9510 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 4.5981 -0.1830 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 3.7320 -1.6830 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 4.5981 -2.1830 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 2.8660 -2.1830 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 4.5981 -3.1830 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 3.7320 -3.6830 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 2.8660 -3.1830 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 5.4641 -3.6830 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 4.9272 2.6270 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 5.6762 0.7344 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 6.0747 1.4246 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 4.5981 1.4370 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 7.5062 2.7800 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 7.7331 3.6270 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 6.8862 3.8539 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 6.3671 3.9930 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 5.5201 4.2200 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 5.2932 3.3730 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 6.2932 1.6410 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 7.1401 1.4140 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 7.3671 2.2610 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 4.8101 -0.7656 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 5.2087 -0.0754 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 3.7320 1.9370 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 5.1350 -1.8730 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 3.7320 -4.3030 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 2.3291 -3.4930 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 5.1541 -4.2200 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 6.0010 -3.9930 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 5.7741 -3.1461 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 1 14 1 0 0 0 0<br> 2 7 1 0 0 0 0<br> 2 34 1 0 0 0 0<br> 3 11 1 0 0 0 0<br> 3 12 1 0 0 0 0<br> 4 5 1 0 0 0 0<br> 4 6 1 0 0 0 0<br> 4 19 1 0 0 0 0<br> 5 8 1 0 0 0 0<br> 5 9 1 0 0 0 0<br> 5 10 1 0 0 0 0<br> 6 7 1 0 0 0 0<br> 6 20 1 0 0 0 0<br> 6 21 1 0 0 0 0<br> 7 11 1 0 0 0 0<br> 7 22 1 0 0 0 0<br> 8 23 1 0 0 0 0<br> 8 24 1 0 0 0 0<br> 8 25 1 0 0 0 0<br> 9 26 1 0 0 0 0<br> 9 27 1 0 0 0 0<br> 9 28 1 0 0 0 0<br> 10 29 1 0 0 0 0<br> 10 30 1 0 0 0 0<br> 10 31 1 0 0 0 0<br> 11 32 1 0 0 0 0<br> 11 33 1 0 0 0 0<br> 12 13 1 0 0 0 0<br> 12 14 2 0 0 0 0<br> 13 15 2 0 0 0 0<br> 13 35 1 0 0 0 0<br> 14 17 1 0 0 0 0<br> 15 16 1 0 0 0 0<br> 15 18 1 0 0 0 0<br> 16 17 2 0 0 0 0<br> 16 36 1 0 0 0 0<br> 17 37 1 0 0 0 0<br> 18 38 1 0 0 0 0<br> 18 39 1 0 0 0 0<br> 18 40 1 0 0 0 0<br>M END
Compound Name
Bupranolol
CID
2475
Molecular Formula
C14H22ClNO2
Molecular Weight
271
No. Hydrogen Bond Acceptors
3
No. Hydrogen Bond Donors
2
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