Synthetic Cannabinoids (Parents) by GC-MS on a ZB-Drug-1

GC Conditions

Column

Zebron ZB-Drug-1, GC Cap. Column 10 m x 0.18 mm x 0.18 µm, Ea

Part No

7CD-G023-08

Phase Name

ZB-Drug-1

Injection

Split 10:1 @ 260°C

Carrier Gas

Constant Flow Helium, 1.2 mL/min

Detection

Mass Selective (MSD) @ (320°C)

Detection Info

Sample Notes

SIM ions: CP47,497(215*,233,318); CP47,497(215*,233,332); HU-210(302,386,330); JWH-073(327,284,310);JWH-073-D7(334,317); JWH-018(341,284,324); JWH-018-D9(350,333); JWH-200(100,384,56)

Sample Preparation Details

Load

Load 2.00 mL Sample diluted in Urine

Wash 1

2 mL 10% Methanol at 2 mL/min

Dry

5 min at greater than 10 inches mercury

Elution 1

4 mL Ethyl acetate: Isopropanol 85:15 at 1 mL/min

Evaporation

Evaporate to dryness

Reconstitute

100 µL Ethyl acetate