Quantification of Carbendazim in Fruit Juice by LC/MS/MS
LC Conditions
Column
Synergi 2.5 µm Fusion-RP 100 Å, LC Column 50 x 2 mm, Ea
Brand
Synergi
Part No
00B-4423-B0
Phase Name
Fusion-RP
Elution Type
Gradient
Mobile Phase
A: 5mM Ammonium Formate in 10% MeOH
B: 5mM Ammonium Formate in 90% MeOH
Gradient Profile
Step No.
Time(min)
%A
%B
1
0
100
0
2
1
100
0
3
15
0
100
4
18
0
100
5
18.05
100
0
6
20
100
0
Flow Rate
0.40 mL/min
Temperature
40°C
Detection
Tandem Mass Spec (MS-MS) @ (22°C)
Detection Info
Sample Notes
SecurityGuard™ ULTRA Guard Cartridge System extends column lifetime. - SecurityGuard ULTRA Cartridges, UHPLC C18 for 2.1mm ID Columns, 3/Pk Part No.: AJ0-8782 - Holder Part No.: AJ0-9000
Order Items Used in This Application
- 1. Carbendazim
-OEChem-05081000422D<br><br> 23 24 0 0 0 0 0 0 0999 V2000<br> 7.7619 -0.6970 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0<br> 6.2619 -1.5630 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0<br> 4.6783 0.9737 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0<br> 4.6783 -0.6357 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0<br> 6.2619 0.1690 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0<br> 3.7320 0.6690 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 3.7320 -0.3310 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 5.2619 0.1690 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 2.8660 1.1690 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 2.8660 -0.8310 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 2.0000 0.6690 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 2.0000 -0.3310 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 6.7619 -0.6970 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 8.2619 -1.5630 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 4.8709 1.5630 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 2.8660 1.7890 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 2.8660 -1.4510 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 1.4631 0.9790 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 1.4631 -0.6410 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 6.5719 0.7059 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 7.7249 -1.8730 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 8.5719 -2.1000 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 8.7988 -1.2530 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 1 13 1 0 0 0 0<br> 1 14 1 0 0 0 0<br> 2 13 2 0 0 0 0<br> 3 6 1 0 0 0 0<br> 3 8 1 0 0 0 0<br> 3 15 1 0 0 0 0<br> 4 7 1 0 0 0 0<br> 4 8 2 0 0 0 0<br> 5 8 1 0 0 0 0<br> 5 13 1 0 0 0 0<br> 5 20 1 0 0 0 0<br> 6 7 1 0 0 0 0<br> 6 9 2 0 0 0 0<br> 7 10 2 0 0 0 0<br> 9 11 1 0 0 0 0<br> 9 16 1 0 0 0 0<br> 10 12 1 0 0 0 0<br> 10 17 1 0 0 0 0<br> 11 12 2 0 0 0 0<br> 11 18 1 0 0 0 0<br> 12 19 1 0 0 0 0<br> 14 21 1 0 0 0 0<br> 14 22 1 0 0 0 0<br> 14 23 1 0 0 0 0<br>M END
Compound Name
Carbendazim
CID
25429
Molecular Formula
C9H9N3O2
Molecular Weight
191
No. Hydrogen Bond Acceptors
3
No. Hydrogen Bond Donors
2
Similar Applications
Reversed Phase
Pesticide panel using Kinetex 2.6u Polar C18 50x4.6mm
Kinetex 2.6 µm Polar C18 100 Å, LC Column 50 x 4.6 mm, Ea
24017
Reversed Phase
185 Pesticides on Kinetex Biphenyl 5u
Kinetex 5 µm Biphenyl 100 Å, LC Column 100 x 2.1 mm, Ea
22618
Reversed Phase
Screening >350 Pesticides from Food & Feed According to Regulation (EC) No. 396/2005
Synergi 2.5 µm Fusion-RP 100 Å, LC Column 50 x 2 mm, Ea
20924
Reversed Phase
Quantification of Carbendazim in Fruit Juice by LC/MS/MS
Synergi 2.5 µm Fusion-RP 100 Å, LC Column 50 x 2 mm, Ea
20568