Food - Quantification of the masked mycotoxin DON-3-glucoside in cereal-based foods by LC/MS/MS

Column

Kinetex 2.6 µm C18 100 Å, LC Column 150 x 2.1 mm, Ea

Brand

Kinetex

Part Number

00F-4462-AN

Phase Name

C18

Elution Type

Gradient

Mobile Phase

A: Water with 0.5% Acetic acid

B: Methanol with 0.5% Acetic acid

Gradient Profile

Step No.

Time(min)

%A

%B

1

0

90

10

2

3

90

10

3

21

60

40

4

27

40

60

5

30

90

10

6

35

90

10

Flow Rate

200.00 mL/min

Temperature

30°C

Detection

Tandem Mass Spec (MS-MS) @ (300°C)

Detection Info

Sample Notes

Michele Suman E-mail address: michele.suman@barilla.com Barilla Food Research Labs, via Mantova 166, 43100 Parma, Italy