LCMS Chiral Separation of Haloxyfop by Lux 3u Cellulose-3
LC Conditions
Column
Lux 3 µm Cellulose-3, LC Column 150 x 4.6 mm, Ea
Brand
Lux
Part No
00F-4492-E0
Phase Name
Cellulose-3
Elution Type
Isocratic
Mobile Phase
A: 0.1% Formic acid/Water
B: ACN
Gradient Profile
Step No.
Time(min)
%A
%B
1
0
55
45
Flow Rate
0.20 mL/min
Temperature
22°C
Detection
Tandem Mass Spec (MS-MS) @ (22°C)
Detection Info
Order Items Used in This Application
- 1. Haloxyfop
- 2. Haloxyfop
-OEChem-05151001052D<br><br> 35 36 0 1 0 0 0 0 0999 V2000<br> 3.7320 3.8770 0.0000 Cl 0 0 0 0 0 0 0 0 0 0 0 0<br> 8.0622 4.3770 0.0000 F 0 0 0 0 0 0 0 0 0 0 0 0<br> 6.6962 4.7430 0.0000 F 0 0 0 0 0 0 0 0 0 0 0 0<br> 7.6962 3.0110 0.0000 F 0 0 0 0 0 0 0 0 0 0 0 0<br> 3.7320 -2.1230 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0<br> 3.7320 1.8770 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0<br> 2.0000 -4.1230 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0<br> 3.7320 -4.1230 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0<br> 5.4641 1.8770 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0<br> 2.8660 -2.6230 0.0000 C 0 0 3 0 0 0 0 0 0 0 0 0<br> 3.7320 -1.1230 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 3.7320 0.8770 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 4.5981 -0.6230 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 2.8660 -0.6230 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 4.5981 0.3770 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 2.8660 0.3770 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 2.0000 -2.1230 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 6.3301 3.3770 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 4.5981 2.3770 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 5.4641 3.8770 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 4.5981 3.3770 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 2.8660 -3.6230 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 6.3301 2.3770 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 7.1962 3.8770 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 2.8660 -2.0030 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 5.1350 -0.9330 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 2.3291 -0.9330 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 5.1350 0.6870 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 2.3291 0.6870 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 2.3100 -1.5861 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 1.4631 -1.8130 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 1.6900 -2.6599 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 5.4641 4.4970 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 6.8671 2.0670 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 2.0000 -4.7430 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 1 21 1 0 0 0 0<br> 2 24 1 0 0 0 0<br> 3 24 1 0 0 0 0<br> 4 24 1 0 0 0 0<br> 5 10 1 0 0 0 0<br> 5 11 1 0 0 0 0<br> 6 12 1 0 0 0 0<br> 6 19 1 0 0 0 0<br> 7 22 1 0 0 0 0<br> 7 35 1 0 0 0 0<br> 8 22 2 0 0 0 0<br> 9 19 1 0 0 0 0<br> 9 23 2 0 0 0 0<br> 10 17 1 0 0 0 0<br> 10 22 1 0 0 0 0<br> 10 25 1 0 0 0 0<br> 11 13 2 0 0 0 0<br> 11 14 1 0 0 0 0<br> 12 15 2 0 0 0 0<br> 12 16 1 0 0 0 0<br> 13 15 1 0 0 0 0<br> 13 26 1 0 0 0 0<br> 14 16 2 0 0 0 0<br> 14 27 1 0 0 0 0<br> 15 28 1 0 0 0 0<br> 16 29 1 0 0 0 0<br> 17 30 1 0 0 0 0<br> 17 31 1 0 0 0 0<br> 17 32 1 0 0 0 0<br> 18 20 2 0 0 0 0<br> 18 23 1 0 0 0 0<br> 18 24 1 0 0 0 0<br> 19 21 2 0 0 0 0<br> 20 21 1 0 0 0 0<br> 20 33 1 0 0 0 0<br> 23 34 1 0 0 0 0<br>M END
Compound Name
Haloxyfop
CID
50895
Molecular Formula
C15H11ClF3NO4
Molecular Weight
361
No. Hydrogen Bond Acceptors
8
No. Hydrogen Bond Donors
1
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