Chiral Separation of Suprofen on Lux 5µm i-Amylose-1 in Ethyl Acetate
LC Conditions
Column
Lux 5 µm i-Amylose-1, LC Column 250 x 4.6 mm, Ea
Brand
Lux
Part No
00G-4762-E0
Phase Name
i-Amylose-1
Elution Type
Isocratic
Mobile Phase
A: 0.1% DEA in Hexane
B: 0.1% TFA in Ethyl acetate
Gradient Profile
Step No.
Time(min)
%A
%B
1
0
70
30
Flow Rate
1.00 mL/min
Temperature
22°C
Detection
UV-Vis Abs.-Variable Wave.(UV) @ (22°C)
Detection Info
Order Items Used in This Application
- 1. Suprofen
- 2. Suprofen
-OEChem-06211003152D<br><br> 30 31 0 1 0 0 0 0 0999 V2000<br> 5.5116 2.1470 0.0000 S 0 0 0 0 0 0 0 0 0 0 0 0<br> 2.8660 -3.4462 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0<br> 2.0000 -1.9462 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0<br> 2.8660 2.5538 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0<br> 3.7320 -1.9462 0.0000 C 0 0 3 0 0 0 0 0 0 0 0 0<br> 3.7320 -0.9462 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 4.5981 -0.4462 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 2.8660 -0.4462 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 3.7320 1.0538 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 4.5981 -2.4462 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 4.5981 0.5538 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 2.8660 0.5538 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 2.8660 -2.4462 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 3.7320 2.0538 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 4.5981 2.5538 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 4.7026 3.5483 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 5.6808 3.7562 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 6.1808 2.8902 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 3.7320 -2.7962 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 5.1350 -0.7562 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 2.3291 -0.7562 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 4.2881 -2.9832 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 5.1350 -2.7562 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 4.9081 -1.9093 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 5.1350 0.8638 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 2.3291 0.8638 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 4.2419 3.9632 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 5.9329 4.3226 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 6.7974 2.8254 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 2.3291 -3.7562 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 1 15 1 0 0 0 0<br> 1 18 1 0 0 0 0<br> 2 13 1 0 0 0 0<br> 2 30 1 0 0 0 0<br> 3 13 2 0 0 0 0<br> 4 14 2 0 0 0 0<br> 5 6 1 0 0 0 0<br> 5 10 1 0 0 0 0<br> 5 13 1 0 0 0 0<br> 5 19 1 0 0 0 0<br> 6 7 2 0 0 0 0<br> 6 8 1 0 0 0 0<br> 7 11 1 0 0 0 0<br> 7 20 1 0 0 0 0<br> 8 12 2 0 0 0 0<br> 8 21 1 0 0 0 0<br> 9 11 2 0 0 0 0<br> 9 12 1 0 0 0 0<br> 9 14 1 0 0 0 0<br> 10 22 1 0 0 0 0<br> 10 23 1 0 0 0 0<br> 10 24 1 0 0 0 0<br> 11 25 1 0 0 0 0<br> 12 26 1 0 0 0 0<br> 14 15 1 0 0 0 0<br> 15 16 2 0 0 0 0<br> 16 17 1 0 0 0 0<br> 16 27 1 0 0 0 0<br> 17 18 2 0 0 0 0<br> 17 28 1 0 0 0 0<br> 18 29 1 0 0 0 0<br>M END
Compound Name
Suprofen
CID
5359
Molecular Formula
C14H12O3S
Molecular Weight
260
No. Hydrogen Bond Acceptors
3
No. Hydrogen Bond Donors
1
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