Children's Sleep Aid Sugar excipients using Luna Omega 3u SUGAR 250x4.6mm - Standards

LC Conditions

Column

Luna Omega 3 µm SUGAR 100 Å, LC Column 250 x 4.6 mm, Ea

Brand

Luna Omega

Part No

00G-4775-E0

Phase Name

SUGAR

Elution Type

Gradient

Mobile Phase

A: 10mM Ammonium Acetate pH 6.4

B: Acetonitrile

Gradient Profile

Step No.

Time(min)

%A

%B

1

0

25

75

2

3

25

75

3

12

40

60

4

14

40

60

5

15

25

75

6

20

25

75

Flow Rate

1.20 mL/min

Temperature

25°C

System

Waters ACQUITY UPLC I-Class Waters ACQUITY UPLC I-Class

Detection

LC/ELSD (Light Scattering) @ (50°C)

Detection Info

Sample Notes

1 pill dissolved in 10mL of Water:Acetonitrile (50:50), Vortex and filtered using Phenex 0.45um Nylon Syringe filter.