Fluconazole Ref Solution A on Kinetex 2.6 µm C18
LC Conditions
Official Method
Ph.Eur. M.2287
Column
Kinetex 2.6 µm C18 100 Å, LC Column 100 x 4.6 mm, Ea
Brand
Kinetex
Part No
00D-4462-E0
Phase Name
C18
Elution Type
Isocratic
Mobile Phase
A: 0.63g/L Ammonium Formate in water
B: Acetonitrile
Gradient Profile
Step No.
Time(min)
%A
%B
1
17
86
14
Flow Rate
1000.00 mL/min
Temperature
40°C
System
Agilent Technologies Agilent Technologies 1260 Infinity
Detection
LC/UV (DAD, PDA) @ 260 nm (nanometers)
Detection Info
Order Items Used in This Application
- 1. Fluconazole
-OEChem-06211003152D<br><br> 34 36 0 0 0 0 0 0 0999 V2000<br> 2.0000 -0.3512 0.0000 F 0 0 0 0 0 0 0 0 0 0 0 0<br> 3.7320 -3.3512 0.0000 F 0 0 0 0 0 0 0 0 0 0 0 0<br> 2.7320 0.6488 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0<br> 4.5981 2.1488 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0<br> 5.5981 0.1488 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0<br> 5.5116 1.7420 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0<br> 5.7026 -0.8457 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0<br> 5.6808 3.3512 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0<br> 7.1808 -0.1876 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0<br> 3.7320 0.6488 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 3.7320 1.6488 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 4.7320 0.6488 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 3.7320 -0.3512 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 2.8660 -0.8512 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 4.5981 -0.8512 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 2.8660 -1.8512 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 4.5981 -1.8512 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 4.7026 3.1433 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 6.5116 0.5555 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 3.7320 -2.3512 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 6.1808 2.4852 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 6.6808 -1.0536 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 3.5200 2.2314 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 3.1215 1.5411 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 5.2070 1.0473 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 4.5716 0.0499 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 2.4220 1.1857 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 5.1350 -0.5412 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 2.3291 -2.1612 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 5.1350 -2.1612 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 4.2419 3.5582 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 6.6405 1.1620 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 6.7974 2.4204 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 6.9329 -1.6200 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 1 14 1 0 0 0 0<br> 2 20 1 0 0 0 0<br> 3 10 1 0 0 0 0<br> 3 27 1 0 0 0 0<br> 4 6 1 0 0 0 0<br> 4 11 1 0 0 0 0<br> 4 18 1 0 0 0 0<br> 5 7 1 0 0 0 0<br> 5 12 1 0 0 0 0<br> 5 19 1 0 0 0 0<br> 6 21 2 0 0 0 0<br> 7 22 2 0 0 0 0<br> 8 18 2 0 0 0 0<br> 8 21 1 0 0 0 0<br> 9 19 2 0 0 0 0<br> 9 22 1 0 0 0 0<br> 10 11 1 0 0 0 0<br> 10 12 1 0 0 0 0<br> 10 13 1 0 0 0 0<br> 11 23 1 0 0 0 0<br> 11 24 1 0 0 0 0<br> 12 25 1 0 0 0 0<br> 12 26 1 0 0 0 0<br> 13 14 2 0 0 0 0<br> 13 15 1 0 0 0 0<br> 14 16 1 0 0 0 0<br> 15 17 2 0 0 0 0<br> 15 28 1 0 0 0 0<br> 16 20 2 0 0 0 0<br> 16 29 1 0 0 0 0<br> 17 20 1 0 0 0 0<br> 17 30 1 0 0 0 0<br> 18 31 1 0 0 0 0<br> 19 32 1 0 0 0 0<br> 21 33 1 0 0 0 0<br> 22 34 1 0 0 0 0<br>M END
Compound Name
Fluconazole
CID
3365
Molecular Formula
C13H12F2N6O
Molecular Weight
306
No. Hydrogen Bond Acceptors
7
No. Hydrogen Bond Donors
1
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