Alprazolam - Alternative Method
LC Conditions
Official Method
USP L10
Column
Luna 3 µm CN 100 Å, LC Column 100 x 4.6 mm, Ea
Brand
Luna
Part No
00D-4254-E0
Phase Name
CN
Elution Type
Isocratic
Mobile Phase
A: Hexane
B: Methylene chloride : Methanol (80:20)
Gradient Profile
Step No.
Time(min)
%A
%B
1
0
75
25
Flow Rate
1.00 mL/min
Temperature
22°C
Detection
UV-Vis Abs.-Variable Wave.(UV) @ (22°C)
Detection Info
Sample Notes
SecurityGuard™ Guard Cartridge System extends column lifetime. - SecurityGuard Cartridges, CN 4 x 3.0mm, 10/Pk Part No.: AJ0-4305 - Holder Part No.: KJ0-4282
Order Items Used in This Application
- 1. Triazolam
- 2. Alprazolam
-OEChem-06211003152D<br><br> 35 38 0 0 0 0 0 0 0999 V2000<br> 2.0000 -0.2812 0.0000 Cl 0 0 0 0 0 0 0 0 0 0 0 0<br> 6.4641 2.2349 0.0000 Cl 0 0 0 0 0 0 0 0 0 0 0 0<br> 5.8374 -1.6082 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0<br> 6.3374 0.5824 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0<br> 7.4235 -1.8947 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0<br> 6.9517 -2.7696 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0<br> 4.9365 -1.1744 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 4.7139 -0.1994 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 6.7384 -1.1744 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 5.3374 0.5824 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 6.9609 -0.1994 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 5.9734 -2.5930 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 4.1839 -1.8946 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 4.9036 1.4834 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 3.7234 0.1229 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 3.1862 -1.5952 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 2.9544 -0.5797 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 5.2518 -3.2853 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 5.4669 2.3096 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 3.9063 1.5581 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 5.0330 3.2106 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 3.4725 2.4591 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 4.0358 3.2853 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 7.5195 -0.4684 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 7.3475 0.2853 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 4.3288 -2.4974 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 3.5925 0.7289 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 2.7334 -2.0187 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 4.8226 -2.8379 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 4.8044 -3.7145 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 5.6811 -3.7327 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 3.5571 1.0458 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 5.3822 3.7228 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 2.8542 2.5054 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 3.7668 3.8439 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 1 17 1 0 0 0 0<br> 2 19 1 0 0 0 0<br> 3 7 1 0 0 0 0<br> 3 9 1 0 0 0 0<br> 3 12 1 0 0 0 0<br> 4 10 2 0 0 0 0<br> 4 11 1 0 0 0 0<br> 5 6 1 0 0 0 0<br> 5 9 2 0 0 0 0<br> 6 12 2 0 0 0 0<br> 7 8 2 0 0 0 0<br> 7 13 1 0 0 0 0<br> 8 10 1 0 0 0 0<br> 8 15 1 0 0 0 0<br> 9 11 1 0 0 0 0<br> 10 14 1 0 0 0 0<br> 11 24 1 0 0 0 0<br> 11 25 1 0 0 0 0<br> 12 18 1 0 0 0 0<br> 13 16 2 0 0 0 0<br> 13 26 1 0 0 0 0<br> 14 19 1 0 0 0 0<br> 14 20 2 0 0 0 0<br> 15 17 2 0 0 0 0<br> 15 27 1 0 0 0 0<br> 16 17 1 0 0 0 0<br> 16 28 1 0 0 0 0<br> 18 29 1 0 0 0 0<br> 18 30 1 0 0 0 0<br> 18 31 1 0 0 0 0<br> 19 21 2 0 0 0 0<br> 20 22 1 0 0 0 0<br> 20 32 1 0 0 0 0<br> 21 23 1 0 0 0 0<br> 21 33 1 0 0 0 0<br> 22 23 2 0 0 0 0<br> 22 34 1 0 0 0 0<br> 23 35 1 0 0 0 0<br>M END
Compound Name
Triazolam
CID
5556
Molecular Formula
C17H12Cl2N4
Molecular Weight
343
No. Hydrogen Bond Acceptors
3
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