Glyburide - USP Method
LC Conditions
Official Method
USP L07
Column
Luna 5 µm C8(2) 100 Å, LC Column 250 x 4.6 mm, Ea
Brand
Luna
Part No
00G-4249-E0
Phase Name
C8(2)
Elution Type
Isocratic
Mobile Phase
A: Acetonitrile
B: 10mM Ammonium phosphate, pH 5.25
Gradient Profile
Step No.
Time(min)
%A
%B
1
0
55
45
Flow Rate
2.00 mL/min
Temperature
22°C
Detection
UV-Vis Abs.-Variable Wave.(UV) @ (22°C)
Detection Info
Sample Notes
SecurityGuard™ Guard Cartridge System extends column lifetime. - SecurityGuard Cartridges, C8 4 x 3.0mm, 10/Pk Part No.: AJ0-4290 - Holder Part No.: KJ0-4282
Order Items Used in This Application
- 1. Glyburide
- 2. Progesterone
-OEChem-06211003152D<br><br> 61 63 0 0 0 0 0 0 0999 V2000<br> 6.3301 -6.7500 0.0000 Cl 0 0 0 0 0 0 0 0 0 0 0 0<br> 6.3301 2.2500 0.0000 S 0 0 0 0 0 0 0 0 0 0 0 0<br> 8.0622 3.2500 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0<br> 7.3301 2.2500 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0<br> 5.3301 2.2500 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0<br> 3.7320 -3.2500 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0<br> 2.8660 -4.7500 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0<br> 7.1962 4.7500 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0<br> 6.3301 3.2500 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0<br> 5.4641 -3.2500 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0<br> 8.0622 5.2500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 8.9282 4.7500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 8.0622 6.2500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 9.7942 5.2500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 8.9282 6.7500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 9.7942 6.2500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 7.1962 3.7500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 6.3301 1.2500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 6.3301 -0.7500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 6.3301 -1.7500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 5.4641 0.7500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 7.1962 0.7500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 5.4641 -0.2500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 7.1962 -0.2500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 5.4641 -2.2500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 4.5981 -3.7500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 4.5981 -4.7500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 3.7320 -5.2500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 5.4641 -5.2500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 3.7320 -6.2500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 5.4641 -6.2500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 4.5981 -6.7500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 2.0000 -5.2500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 8.0622 4.6300 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 8.5297 4.2750 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 9.3267 4.2750 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 7.8501 6.8326 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 7.4516 6.1423 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 10.0063 4.6674 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 10.4048 5.3577 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 9.3267 7.2250 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 8.5297 7.2250 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 10.4048 6.1423 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 10.0063 6.8326 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 6.6592 5.0600 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 5.7932 3.5600 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 6.5422 -2.3326 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 6.9407 -1.6423 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 4.9272 1.0600 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 7.7331 1.0600 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 4.9272 -0.5600 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 7.7331 -0.5600 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 5.2520 -1.6674 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 4.8535 -2.3577 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 6.0010 -3.5600 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 6.0010 -4.9400 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 3.1951 -6.5600 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 4.5981 -7.3700 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 1.6900 -4.7131 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 1.4631 -5.5600 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 2.3100 -5.7869 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 1 31 1 0 0 0 0<br> 2 4 2 0 0 0 0<br> 2 5 2 0 0 0 0<br> 2 9 1 0 0 0 0<br> 2 18 1 0 0 0 0<br> 3 17 2 0 0 0 0<br> 6 26 2 0 0 0 0<br> 7 28 1 0 0 0 0<br> 7 33 1 0 0 0 0<br> 8 11 1 0 0 0 0<br> 8 17 1 0 0 0 0<br> 8 45 1 0 0 0 0<br> 9 17 1 0 0 0 0<br> 9 46 1 0 0 0 0<br> 10 25 1 0 0 0 0<br> 10 26 1 0 0 0 0<br> 10 55 1 0 0 0 0<br> 11 12 1 0 0 0 0<br> 11 13 1 0 0 0 0<br> 11 34 1 0 0 0 0<br> 12 14 1 0 0 0 0<br> 12 35 1 0 0 0 0<br> 12 36 1 0 0 0 0<br> 13 15 1 0 0 0 0<br> 13 37 1 0 0 0 0<br> 13 38 1 0 0 0 0<br> 14 16 1 0 0 0 0<br> 14 39 1 0 0 0 0<br> 14 40 1 0 0 0 0<br> 15 16 1 0 0 0 0<br> 15 41 1 0 0 0 0<br> 15 42 1 0 0 0 0<br> 16 43 1 0 0 0 0<br> 16 44 1 0 0 0 0<br> 18 21 2 0 0 0 0<br> 18 22 1 0 0 0 0<br> 19 20 1 0 0 0 0<br> 19 23 2 0 0 0 0<br> 19 24 1 0 0 0 0<br> 20 25 1 0 0 0 0<br> 20 47 1 0 0 0 0<br> 20 48 1 0 0 0 0<br> 21 23 1 0 0 0 0<br> 21 49 1 0 0 0 0<br> 22 24 2 0 0 0 0<br> 22 50 1 0 0 0 0<br> 23 51 1 0 0 0 0<br> 24 52 1 0 0 0 0<br> 25 53 1 0 0 0 0<br> 25 54 1 0 0 0 0<br> 26 27 1 0 0 0 0<br> 27 28 2 0 0 0 0<br> 27 29 1 0 0 0 0<br> 28 30 1 0 0 0 0<br> 29 31 2 0 0 0 0<br> 29 56 1 0 0 0 0<br> 30 32 2 0 0 0 0<br> 30 57 1 0 0 0 0<br> 31 32 1 0 0 0 0<br> 32 58 1 0 0 0 0<br> 33 59 1 0 0 0 0<br> 33 60 1 0 0 0 0<br> 33 61 1 0 0 0 0<br>M END
Compound Name
Glyburide
CID
3488
Molecular Formula
C23H28ClN3O5S
Molecular Weight
494
No. Hydrogen Bond Acceptors
5
No. Hydrogen Bond Donors
3
Similar Applications
Reversed Phase
Glyburide - USP Method
Luna 5 µm C8(2) 100 Å, LC Column 250 x 4.6 mm, Ea
3316