EPA Method 8330: Explosive Mix Using Synergi Hydro-RP
LC Conditions
Column
Synergi 4 µm Hydro-RP 80 Å, LC Column 250 x 4.6 mm, Ea
Brand
Synergi
Part No
00G-4375-E0
Phase Name
Hydro-RP
Elution Type
Gradient
Mobile Phase
A: Methanol
B: Water
Gradient Profile
Step No.
Time(min)
%A
%B
1
0
55
45
2
2
55
45
3
22
75
25
4
22.01
55
45
5
25
55
45
Flow Rate
1.00 mL/min
Temperature
35°C
Detection
UV-Vis Abs.-Variable Wave.(UV) @ (22°C)
Detection Info
Sample Notes
100ul of 100ug/ml 17 component mix was diluted with 900ul of 50:50 Methanol/water
Order Items Used in This Application
- 1. Octahydro-1,3,5,7-tetranitro-1,3,5,7-tetrazocine (HMX)
- 2. Hexahydro-1,3,5-trinitro-1,3,5-triazine
- 3. 1,3,5-Trinitrobenzene
- 4. Methyl-2,4,6-trinitrophenylnitramine (Tetryl)
- 5. 1,3-Dinitrobenzene
- 6. Nitrobenzene
- 7. Nitroglycerin
- 8. 2,4,6-Trinitrotoluene
- 9. 3,5-Dinitroaniline
- 10. 4-Amino-2,6 dinitrotoluene
- 11. 2 Amino-4,6 dinitrotoluene
- 12. 2,6-Dinitrotoluene
- 13. 2,4-Dinitrotoluene
- 14. Pentaerythritol tetranitrate
- 15. 2-Nitrotoluene
- 16. 4-Nitrotoluene
- 17. 3-Nitrotoluene
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