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Applications
Calibration Curve for Melamine Extraction (20-2000ng/mL range) from Strata Melamine on Luna HILIC
18467
Separation Mode: Hydrophilic Interaction
Hydrophilic Interaction
HILIC
HPLC
Pollutant / Contaminant
Environmental / Health

Calibration Curve for Melamine Extraction (20-2000ng/mL range) from Strata Melamine on Luna HILIC

Analytes
1Melamine
2Melamine 13C3-Amino 15N3
Details
LC Conditions (App ID: 18467)
Column:
Brand Name:
Luna
Part No:
Phase Name:
HILIC
Sample Note:
LC/MS/MS Condition: Column: Luna 3µm HILIC, 100x2.0mm; Flow rate: 0.4ml/min Mobile Phase: Isocratic; 90/10 ACN/100mM NH4 Formate pH 3.2; MS Detector: API 3000 LC/MS/MS with ESI (TurboIonSpray®) (www.Appliedbiosystems.com), Switch from -ve Ion Mode (for cyanuric) to Positive Ion (for Melamine); MRM; heater gas flow 7000 cc/min; heater temperature 450 °C Melamine QC - 200 ng % Accuracy 99.45% % CV 6% Calibration Curve of Extracted Samples conc. (ng) % Accuracy 20 102% 40 96% 200 104% 400 98% 2000 100.03%
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