1Melamine |
---|
2Melamine 13C3-Amino 15N3 |
1Melamine |
---|
2Melamine 13C3-Amino 15N3 |
Column: |
Brand Name: Luna |
Part No: |
Phase Name: HILIC |
Sample Note: LC/MS/MS Condition:
Column: Luna 3µm HILIC, 100x2.0mm; Flow rate: 0.4ml/min
Mobile Phase: Isocratic; 90/10 ACN/100mM NH4 Formate pH 3.2; MS Detector: API 3000 LC/MS/MS with ESI (TurboIonSpray®) (www.Appliedbiosystems.com), Switch from -ve Ion Mode (for cyanuric) to Positive Ion (for Melamine);
MRM; heater gas flow 7000 cc/min; heater temperature 450 °C
Melamine QC - 200 ng
% Accuracy 99.45%
% CV 6%
Calibration Curve of Extracted Samples
conc. (ng) % Accuracy
20 102%
40 96%
200 104%
400 98%
2000 100.03% |