b-Blockers (Toliprolol) on Lux 5 µm Cellulose-1 by Chiral SFC
LC Conditions
Column
Lux 5 µm Cellulose-1, LC Column 250 x 4.6 mm, Ea
Brand
Lux
Part No
00G-4459-E0
Phase Name
Cellulose-1
Elution Type
Isocratic
Mobile Phase
A: Methanol with 0.1% DEA
B: Carbon Dioxide
Gradient Profile
Step No.
Time(min)
%A
%B
1
0
20
80
Flow Rate
1.00 mL/min
Temperature
35°C
Detection
UV-Vis Abs.-Diode Array (PDA) @ (22°C)
Detection Info
Sample Notes
Application using Jasco SFC instrument courtesy of Cephalon, Inc.
Order Items Used in This Application
- 1. Toliprolol
- 2. Toliprolol
-OEChem-06211003152D<br><br> 37 37 0 1 0 0 0 0 0999 V2000<br> 3.7320 -0.7500 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0<br> 3.7320 1.2500 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0<br> 5.4641 2.2500 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0<br> 5.4641 1.2500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 4.5981 0.7500 0.0000 C 0 0 3 0 0 0 0 0 0 0 0 0<br> 6.3301 2.7500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 4.5981 -0.2500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 6.3301 3.7500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 7.1962 2.2500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 3.7320 -1.7500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 2.8660 -2.2500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 2.8660 -3.2500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 4.5981 -2.2500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 3.7320 -3.7500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 4.5981 -3.2500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 2.0000 -3.7500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0<br> 5.6762 0.6674 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 6.0747 1.3577 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 4.5981 1.3700 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 5.7932 3.0600 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 4.9272 2.5600 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 4.8101 -0.8326 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 5.2087 -0.1423 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 6.9501 3.7500 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 6.3301 4.3700 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 5.7101 3.7500 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 6.8862 1.7131 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 7.7331 1.9400 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 7.5062 2.7869 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 3.7320 1.8700 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 2.3291 -1.9400 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 5.1350 -1.9400 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 3.7320 -4.3700 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 5.1350 -3.5600 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 1.6900 -3.2131 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 1.4631 -4.0600 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 2.3100 -4.2869 0.0000 H 0 0 0 0 0 0 0 0 0 0 0 0<br> 1 7 1 0 0 0 0<br> 1 10 1 0 0 0 0<br> 2 5 1 0 0 0 0<br> 2 30 1 0 0 0 0<br> 3 4 1 0 0 0 0<br> 3 6 1 0 0 0 0<br> 3 21 1 0 0 0 0<br> 4 5 1 0 0 0 0<br> 4 17 1 0 0 0 0<br> 4 18 1 0 0 0 0<br> 5 7 1 0 0 0 0<br> 5 19 1 0 0 0 0<br> 6 8 1 0 0 0 0<br> 6 9 1 0 0 0 0<br> 6 20 1 0 0 0 0<br> 7 22 1 0 0 0 0<br> 7 23 1 0 0 0 0<br> 8 24 1 0 0 0 0<br> 8 25 1 0 0 0 0<br> 8 26 1 0 0 0 0<br> 9 27 1 0 0 0 0<br> 9 28 1 0 0 0 0<br> 9 29 1 0 0 0 0<br> 10 11 1 0 0 0 0<br> 10 13 2 0 0 0 0<br> 11 12 2 0 0 0 0<br> 11 31 1 0 0 0 0<br> 12 14 1 0 0 0 0<br> 12 16 1 0 0 0 0<br> 13 15 1 0 0 0 0<br> 13 32 1 0 0 0 0<br> 14 15 2 0 0 0 0<br> 14 33 1 0 0 0 0<br> 15 34 1 0 0 0 0<br> 16 35 1 0 0 0 0<br> 16 36 1 0 0 0 0<br> 16 37 1 0 0 0 0<br>M END
Compound Name
Toliprolol
CID
18047
Molecular Formula
C13H21NO2
Molecular Weight
223
No. Hydrogen Bond Acceptors
3
No. Hydrogen Bond Donors
2
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