Quantification of Organophosphorus Pesticides by QuEchERS and LC/MS/MS
LC Conditions
Column
Synergi 4 µm Fusion-RP 80 Å, LC Column 50 x 2 mm, Ea
Brand
Synergi
Part No
00B-4424-B0
Phase Name
Fusion-RP
Elution Type
Gradient
Mobile Phase
A: Add 5mL of 1M ammonium formate to 1L Water
B: Add 5mL of 1M ammonium formate to 1L Methanol
Gradient Profile
Step No.
Time(min)
%A
%B
1
-5
95
5
2
0
95
5
3
2
95
5
4
6
50
50
5
12
10
90
6
14
10
90
7
16
95
5
8
17
95
5
Flow Rate
250.00 mL/min
Temperature
25°C
Detection
Tandem Mass Spec (MS-MS) @ (22°C)
Detection Info
Sample Notes
SecurityGuard™ Guard Cartridge System extends column lifetime. - SecurityGuard Cartridges, Fusion-RP 4 x 2.0mm ID, 10/Pk Part No.: AJ0-7556 - Holder Part No.: KJ0-4282
Order Items Used in This Application
- 1. Acephate
- 2. Acephate
- 3. Demeton-S-methyl sulfone
- 4. Demeton-S-methyl sulfone
- 5. Parathion-methyl
- 6. Parathion-methyl
- 7. Dicrotophos
- 8. Dicrotophos
- 9. Demeton-S-methyl
- 10. Demeton-S-methyl
- 11. Dimethoate
- 12. Dimethoate
- 13. Mevinphos
- 14. Mevinphos
- 15. Dichlorvos
- 16. Dichlorvos
- 17. Phorate sulfoxide
- 18. Phorate sulfoxide
- 19. Famphur
- 20. Famphur
- 21. Naled
- 22. Naled
- 23. Azinphos-methyl
- 24. Azinphos-methyl
- 25. Malathion
- 26. Malathion
- 27. Triazophos
- 28. Triazophos
- 29. Azinphos-ethyl
- 30. Azinphos-ethyl
- 31. Tetrachlorvinphos
- 32. Tetrachlorvinphos
- 33. EPTC
- 34. EPTC
- 35. Chlorfenvinphos
- 36. Chlorfenvinphos
- 37. Parathion
- 38. Parathion
- 39. Sulfotep
- 40. Sulfotep
- 41. Diazinon
- 42. Diazinon
- 43. Fenthion
- 44. Fenthion
- 45. Coumaphos
- 46. Coumaphos
- 47. Phorate
- 48. Phorate
- 49. Pirimiphos-methyl
- 50. Pirimiphos-methyl
- 51. Pirimiphos-ethyl
- 52. Pirimiphos-ethyl
- 53. Sulprofos
- 54. Sulprofos
- 55. Chlorpyrifos
- 56. Chlorpyrifos
- 57. Tokuthion
- 58. Tokuthion
Similar Applications
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