Hexobarbital on Lux 5µm Cellulose-4 by SFC

LC Conditions

Column

Lux 5 µm Cellulose-4, LC Column 250 x 4.6 mm, Ea

Brand

Lux

Part No

00G-4491-E0

Phase Name

Cellulose-4

Elution Type

Isocratic

Mobile Phase

A: CO2/(Isopropanol + 0.25% IPA + 0.25% TFA) 90:10 (v/v)

Gradient Profile

Step No.

Time(min)

100

Flow Rate

3.00 mL/min

Temperature

30°C

Detection

UV-Vis Abs.-Diode Array (PDA) @ (30°C)

Detection Info

Sample Notes

Courtesy of Katrijn De Klerck, Debby Mangelings and Yvan Vander Heyden, Department of Analytical Chemistry and Pharmaceutical Technology, Vrije Universiteit Brussel, Brussels, Belgium. Results of this analysis yielded: Alpha >1.1 and Resolution >1.5 SecurityGuard™ Guard Cartridge System extends column lifetime. - SecurityGuard Cartridges, Lux Cellulose-4, 4 x 3.0mm ID, 10/Pk Part No.: AJ0-8627 - Holder Part No.: KJ0-4282

Order Items Used in This Application

00G-4491-E0

Lux 5 µm Cellulose-4, LC Column 250 x 4.6 mm, Ea

View Product

1. Hexobarbital
2. Hexobarbital

-OEChem-06211003152D<br><br> 33 34  0     1  0  0  0  0  0999 V2000<br>    2.0000    0.2010    0.0000 O   0  0  0  0  0  0  0  0  0  0  0  0<br>    5.4641    0.2010    0.0000 O   0  0  0  0  0  0  0  0  0  0  0  0<br>    3.7320   -2.7990    0.0000 O   0  0  0  0  0  0  0  0  0  0  0  0<br>    2.8660   -1.2990    0.0000 N   0  0  0  0  0  0  0  0  0  0  0  0<br>    4.5981   -1.2990    0.0000 N   0  0  0  0  0  0  0  0  0  0  0  0<br>    3.7320    0.2010    0.0000 C   0  0  3  0  0  0  0  0  0  0  0  0<br>    4.2320    1.0670    0.0000 C   0  0  0  0  0  0  0  0  0  0  0  0<br>    5.2320    1.0670    0.0000 C   0  0  0  0  0  0  0  0  0  0  0  0<br>    5.7320    1.9330    0.0000 C   0  0  0  0  0  0  0  0  0  0  0  0<br>    5.2320    2.7990    0.0000 C   0  0  0  0  0  0  0  0  0  0  0  0<br>    4.2320    2.7990    0.0000 C   0  0  0  0  0  0  0  0  0  0  0  0<br>    3.7320    1.9330    0.0000 C   0  0  0  0  0  0  0  0  0  0  0  0<br>    2.8660   -0.2990    0.0000 C   0  0  0  0  0  0  0  0  0  0  0  0<br>    3.2320    1.0670    0.0000 C   0  0  0  0  0  0  0  0  0  0  0  0<br>    4.5981   -0.2990    0.0000 C   0  0  0  0  0  0  0  0  0  0  0  0<br>    3.7320   -1.7990    0.0000 C   0  0  0  0  0  0  0  0  0  0  0  0<br>    2.0000   -1.7990    0.0000 C   0  0  0  0  0  0  0  0  0  0  0  0<br>    5.1244    0.4564    0.0000 H   0  0  0  0  0  0  0  0  0  0  0  0<br>    5.8147    0.8549    0.0000 H   0  0  0  0  0  0  0  0  0  0  0  0<br>    6.2070    1.5345    0.0000 H   0  0  0  0  0  0  0  0  0  0  0  0<br>    6.2070    2.3315    0.0000 H   0  0  0  0  0  0  0  0  0  0  0  0<br>    5.8147    3.0111    0.0000 H   0  0  0  0  0  0  0  0  0  0  0  0<br>    5.1244    3.4096    0.0000 H   0  0  0  0  0  0  0  0  0  0  0  0<br>    4.3397    3.4096    0.0000 H   0  0  0  0  0  0  0  0  0  0  0  0<br>    3.6494    3.0111    0.0000 H   0  0  0  0  0  0  0  0  0  0  0  0<br>    3.1120    1.9330    0.0000 H   0  0  0  0  0  0  0  0  0  0  0  0<br>    3.7690    1.3770    0.0000 H   0  0  0  0  0  0  0  0  0  0  0  0<br>    2.9220    1.6039    0.0000 H   0  0  0  0  0  0  0  0  0  0  0  0<br>    2.6951    0.7570    0.0000 H   0  0  0  0  0  0  0  0  0  0  0  0<br>    5.1350   -1.6090    0.0000 H   0  0  0  0  0  0  0  0  0  0  0  0<br>    1.6900   -1.2621    0.0000 H   0  0  0  0  0  0  0  0  0  0  0  0<br>    1.4631   -2.1090    0.0000 H   0  0  0  0  0  0  0  0  0  0  0  0<br>    2.3100   -2.3360    0.0000 H   0  0  0  0  0  0  0  0  0  0  0  0<br>  1 13  2  0  0  0  0<br>  2 15  2  0  0  0  0<br>  3 16  2  0  0  0  0<br>  4 13  1  0  0  0  0<br>  4 16  1  0  0  0  0<br>  4 17  1  0  0  0  0<br>  5 15  1  0  0  0  0<br>  5 16  1  0  0  0  0<br>  5 30  1  0  0  0  0<br>  6  7  1  0  0  0  0<br>  6 13  1  0  0  0  0<br>  6 14  1  0  0  0  0<br>  6 15  1  0  0  0  0<br>  7  8  1  0  0  0  0<br>  7 12  2  0  0  0  0<br>  8  9  1  0  0  0  0<br>  8 18  1  0  0  0  0<br>  8 19  1  0  0  0  0<br>  9 10  1  0  0  0  0<br>  9 20  1  0  0  0  0<br>  9 21  1  0  0  0  0<br> 10 11  1  0  0  0  0<br> 10 22  1  0  0  0  0<br> 10 23  1  0  0  0  0<br> 11 12  1  0  0  0  0<br> 11 24  1  0  0  0  0<br> 11 25  1  0  0  0  0<br> 12 26  1  0  0  0  0<br> 14 27  1  0  0  0  0<br> 14 28  1  0  0  0  0<br> 14 29  1  0  0  0  0<br> 17 31  1  0  0  0  0<br> 17 32  1  0  0  0  0<br> 17 33  1  0  0  0  0<br>M  END

Compound Name

Hexobarbital

CID

3608

Molecular Formula

C12H16N2O3

Molecular Weight

236

No. Hydrogen Bond Acceptors

No. Hydrogen Bond Donors

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