Neonicotinoids honey extract by LC/MS/MS using roQ and Kinetex Biphenyl

LC Conditions

Column

Kinetex 2.6 µm Biphenyl 100 Å, LC Column 50 x 2.1 mm, Ea

Brand

Kinetex

Part No

00B-4622-AN

Phase Name

Biphenyl

Elution Type

Gradient

Mobile Phase

A: 0.1% Formic acid in water

B: 0.1% Formic acid in acetonitrile

Gradient Profile

Step No.

Time(min)

%A

%B

1

0

95

5

2

10

30

70

3

12

30

70

4

12.1

95

5

5

14.1

95

5

Flow Rate

0.50 mL/min

Temperature

22°C

Detection

Tandem Mass Spec (MS-MS) @ (22°C)

Detection Info