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Applications
LC-MS/MS Pesticides ( simazine ) - RC Filter in Cumin Exacts for the comparison of with/without Filter Vial-- clone
26539
Separation Mode: Reversed Phase
Reversed Phase
C18
HPLC
Food & Beverage
Pesticide / Insecticide
Environmental / Health

LC-MS/MS Pesticides ( simazine ) - RC Filter in Cumin Exacts for the comparison of with/without Filter Vial-- clone

Analytes
1simazine
2simazine
Compound Name
Cid42
CID
42
Molecular Formula
C9H10O6
Molecular Weight
214
No. Hydrogen Bond Acceptors
6
No. Hydrogen Bond Donors
3
Details
LC Conditions (App ID: 26539)
Column:
Brand Name:
Part No:
Phase Name:
C18
Elution Type:
Gradient
Mobile Phase:
A: 0.1% Formic Acid and 10mM Ammonium Acetate in water
B: 0.5% Formic Acid in Methanol
Gradient Profile:
Step No.Time(min)%A%B
10955
20.1955
30.54060
43.52575
581585
610.5595
712595
812.1955
918955
Flow Rate:
0.4 mL/min
Temperature:
20°C
System:
Agilent Technologies 1100 Series Agilent Technologies 1100 Series
Detection:
LC/MS/MS
Sample Note:
a) Prepared 1mg/mL simazine solutions with other 17 pesticide standards b) Take sample to prepare a 10x Diluted mixture by placing 100uL of the existing mix into a 900uL of a 1:2 Water:Acetonitrile mix. c) Place 30uL of the 10x diluted mixture into 270 uL of the chili powder supernatant. d) Place 450uL of sample from step c) into the filter vial for final analysis.

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