USP Plerixafor Injection: Assay and Organic Impurities- std sol assay

LC Conditions
Column

Luna 5 µm C18(2) 100 Å, LC Column 250 x 4.6 mm, Ea

Brand

Luna

Part No

00G-4252-E0

Phase Name

C18(2)

Elution Type

Gradient

Mobile Phase

A: Methanol + Water + TFA (8.5:91.5:1)

B: Methanol + Water + TFA (50:50:1)

Gradient Profile

Step No.

Time(min)

%A

%B

1

0

100

0

2

20

100

0

3

32

48

52

4

33

10

90

5

34

10

90

6

34.1

100

0

7

40

100

0

Flow Rate

1.00 mL/min

Temperature

45°C

System

Agilent Technologies 1260 Infinity Agilent Technologies 1260 Infinity

Detection

LC/UV (DAD, PDA) @ 230 nm (nanometers)

Detection Info
Sample Notes

Standard Solution Assay (2mg/mL Plerixafor RS in diluent)

Order Items Used in This Application

Luna 5 µm C18(2) 100 Å, LC Column 250 x 4.6 mm, Ea
00G-4252-E0

Luna 5 µm C18(2) 100 Å, LC Column 250 x 4.6 mm, Ea

View Product

  • 1. Plerixafor
-OEChem-05151001062D<br><br> 90 92  0     1  0  0  0  0  0999 V2000<br>    6.1200    1.7320    0.0000 N   0  0  3  0  0  0  0  0  0  0  0  0<br>   10.1200   -1.7320    0.0000 N   0  0  3  0  0  0  0  0  0  0  0  0<br>    4.1200    0.0000    0.0000 N   0  0  0  0  0  0  0  0  0  0  0  0<br>   12.1200    0.0000    0.0000 N   0  0  0  0  0  0  0  0  0  0  0  0<br>    4.6200    4.3301    0.0000 N   0  0  0  0  0  0  0  0  0  0  0  0<br>   11.6200   -4.3301    0.0000 N   0  0  0  0  0  0  0  0  0  0  0  0<br>    2.6200    2.5981    0.0000 N   0  0  0  0  0  0  0  0  0  0  0  0<br>   13.6200   -2.5981    0.0000 N   0  0  0  0  0  0  0  0  0  0  0  0<br>    5.6200    2.5981    0.0000 C   0  0  0  0  0  0  0  0  0  0  0  0<br>   10.6200   -2.5981    0.0000 C   0  0  0  0  0  0  0  0  0  0  0  0<br>    7.1200    1.7320    0.0000 C   0  0  0  0  0  0  0  0  0  0  0  0<br>    9.1200   -1.7320    0.0000 C   0  0  0  0  0  0  0  0  0  0  0  0<br>    5.6200    0.8660    0.0000 C   0  0  0  0  0  0  0  0  0  0  0  0<br>   10.6200   -0.8660    0.0000 C   0  0  0  0  0  0  0  0  0  0  0  0<br>    6.1200    3.4641    0.0000 C   0  0  0  0  0  0  0  0  0  0  0  0<br>   10.1200   -3.4641    0.0000 C   0  0  0  0  0  0  0  0  0  0  0  0<br>    7.6200    0.8660    0.0000 C   0  0  0  0  0  0  0  0  0  0  0  0<br>    8.6200   -0.8660    0.0000 C   0  0  0  0  0  0  0  0  0  0  0  0<br>    4.6200    0.8660    0.0000 C   0  0  0  0  0  0  0  0  0  0  0  0<br>   11.6200   -0.8660    0.0000 C   0  0  0  0  0  0  0  0  0  0  0  0<br>    5.6200    4.3301    0.0000 C   0  0  0  0  0  0  0  0  0  0  0  0<br>   10.6200   -4.3301    0.0000 C   0  0  0  0  0  0  0  0  0  0  0  0<br>    8.6200    0.8660    0.0000 C   0  0  0  0  0  0  0  0  0  0  0  0<br>    9.1200    0.0000    0.0000 C   0  0  0  0  0  0  0  0  0  0  0  0<br>    7.1200    0.0000    0.0000 C   0  0  0  0  0  0  0  0  0  0  0  0<br>    7.6200   -0.8660    0.0000 C   0  0  0  0  0  0  0  0  0  0  0  0<br>    3.1200    0.0000    0.0000 C   0  0  0  0  0  0  0  0  0  0  0  0<br>   13.1200    0.0000    0.0000 C   0  0  0  0  0  0  0  0  0  0  0  0<br>    2.6200    0.8660    0.0000 C   0  0  0  0  0  0  0  0  0  0  0  0<br>   13.6200   -0.8660    0.0000 C   0  0  0  0  0  0  0  0  0  0  0  0<br>    4.1200    3.4641    0.0000 C   0  0  0  0  0  0  0  0  0  0  0  0<br>   12.1200   -3.4641    0.0000 C   0  0  0  0  0  0  0  0  0  0  0  0<br>    3.1200    1.7320    0.0000 C   0  0  0  0  0  0  0  0  0  0  0  0<br>   13.1200   -1.7320    0.0000 C   0  0  0  0  0  0  0  0  0  0  0  0<br>    3.1200    3.4641    0.0000 C   0  0  0  0  0  0  0  0  0  0  0  0<br>   13.1200   -3.4641    0.0000 C   0  0  0  0  0  0  0  0  0  0  0  0<br>    5.1450    2.9966    0.0000 H   0  0  0  0  0  0  0  0  0  0  0  0<br>    5.1450    2.1996    0.0000 H   0  0  0  0  0  0  0  0  0  0  0  0<br>   11.0949   -2.9966    0.0000 H   0  0  0  0  0  0  0  0  0  0  0  0<br>   11.0949   -2.1996    0.0000 H   0  0  0  0  0  0  0  0  0  0  0  0<br>    7.7026    1.9441    0.0000 H   0  0  0  0  0  0  0  0  0  0  0  0<br>    7.0123    2.3426    0.0000 H   0  0  0  0  0  0  0  0  0  0  0  0<br>    8.5374   -1.9441    0.0000 H   0  0  0  0  0  0  0  0  0  0  0  0<br>    9.2277   -2.3426    0.0000 H   0  0  0  0  0  0  0  0  0  0  0  0<br>    5.5123    0.2554    0.0000 H   0  0  0  0  0  0  0  0  0  0  0  0<br>    6.2026    0.6540    0.0000 H   0  0  0  0  0  0  0  0  0  0  0  0<br>   10.7277   -0.2554    0.0000 H   0  0  0  0  0  0  0  0  0  0  0  0<br>   10.0374   -0.6540    0.0000 H   0  0  0  0  0  0  0  0  0  0  0  0<br>    6.5950    3.0656    0.0000 H   0  0  0  0  0  0  0  0  0  0  0  0<br>    6.5950    3.8626    0.0000 H   0  0  0  0  0  0  0  0  0  0  0  0<br>    9.6450   -3.0656    0.0000 H   0  0  0  0  0  0  0  0  0  0  0  0<br>    9.6450   -3.8626    0.0000 H   0  0  0  0  0  0  0  0  0  0  0  0<br>    4.7277    1.4766    0.0000 H   0  0  0  0  0  0  0  0  0  0  0  0<br>    4.0374    1.0781    0.0000 H   0  0  0  0  0  0  0  0  0  0  0  0<br>   11.5123   -1.4766    0.0000 H   0  0  0  0  0  0  0  0  0  0  0  0<br>   12.2026   -1.0781    0.0000 H   0  0  0  0  0  0  0  0  0  0  0  0<br>    6.2026    4.5422    0.0000 H   0  0  0  0  0  0  0  0  0  0  0  0<br>    5.5123    4.9407    0.0000 H   0  0  0  0  0  0  0  0  0  0  0  0<br>   10.0374   -4.5422    0.0000 H   0  0  0  0  0  0  0  0  0  0  0  0<br>   10.7277   -4.9407    0.0000 H   0  0  0  0  0  0  0  0  0  0  0  0<br>    8.9300    1.4030    0.0000 H   0  0  0  0  0  0  0  0  0  0  0  0<br>    9.7400    0.0000    0.0000 H   0  0  0  0  0  0  0  0  0  0  0  0<br>    6.5000    0.0000    0.0000 H   0  0  0  0  0  0  0  0  0  0  0  0<br>    7.3100   -1.4030    0.0000 H   0  0  0  0  0  0  0  0  0  0  0  0<br>    4.4300   -0.5369    0.0000 H   0  0  0  0  0  0  0  0  0  0  0  0<br>   11.8100    0.5369    0.0000 H   0  0  0  0  0  0  0  0  0  0  0  0<br>    2.5374   -0.2121    0.0000 H   0  0  0  0  0  0  0  0  0  0  0  0<br>    3.2277   -0.6106    0.0000 H   0  0  0  0  0  0  0  0  0  0  0  0<br>   13.7026    0.2121    0.0000 H   0  0  0  0  0  0  0  0  0  0  0  0<br>   13.0123    0.6106    0.0000 H   0  0  0  0  0  0  0  0  0  0  0  0<br>    2.1450    1.2646    0.0000 H   0  0  0  0  0  0  0  0  0  0  0  0<br>    2.1450    0.4675    0.0000 H   0  0  0  0  0  0  0  0  0  0  0  0<br>   14.0949   -1.2646    0.0000 H   0  0  0  0  0  0  0  0  0  0  0  0<br>   14.0949   -0.4675    0.0000 H   0  0  0  0  0  0  0  0  0  0  0  0<br>    4.3100    4.8671    0.0000 H   0  0  0  0  0  0  0  0  0  0  0  0<br>   11.9300   -4.8671    0.0000 H   0  0  0  0  0  0  0  0  0  0  0  0<br>    4.0123    2.8535    0.0000 H   0  0  0  0  0  0  0  0  0  0  0  0<br>    4.7026    3.2520    0.0000 H   0  0  0  0  0  0  0  0  0  0  0  0<br>   12.2277   -2.8535    0.0000 H   0  0  0  0  0  0  0  0  0  0  0  0<br>   11.5374   -3.2520    0.0000 H   0  0  0  0  0  0  0  0  0  0  0  0<br>    3.5950    1.3335    0.0000 H   0  0  0  0  0  0  0  0  0  0  0  0<br>    3.5950    2.1306    0.0000 H   0  0  0  0  0  0  0  0  0  0  0  0<br>   12.6451   -1.3335    0.0000 H   0  0  0  0  0  0  0  0  0  0  0  0<br>   12.6451   -2.1306    0.0000 H   0  0  0  0  0  0  0  0  0  0  0  0<br>    3.2277    4.0747    0.0000 H   0  0  0  0  0  0  0  0  0  0  0  0<br>    2.5374    3.6762    0.0000 H   0  0  0  0  0  0  0  0  0  0  0  0<br>   13.0123   -4.0747    0.0000 H   0  0  0  0  0  0  0  0  0  0  0  0<br>   13.7026   -3.6762    0.0000 H   0  0  0  0  0  0  0  0  0  0  0  0<br>    2.0000    2.5981    0.0000 H   0  0  0  0  0  0  0  0  0  0  0  0<br>   14.2400   -2.5981    0.0000 H   0  0  0  0  0  0  0  0  0  0  0  0<br>  1  9  1  0  0  0  0<br>  1 11  1  0  0  0  0<br>  1 13  1  0  0  0  0<br>  2 10  1  0  0  0  0<br>  2 12  1  0  0  0  0<br>  2 14  1  0  0  0  0<br>  3 19  1  0  0  0  0<br>  3 27  1  0  0  0  0<br>  3 65  1  0  0  0  0<br>  4 20  1  0  0  0  0<br>  4 28  1  0  0  0  0<br>  4 66  1  0  0  0  0<br>  5 21  1  0  0  0  0<br>  5 31  1  0  0  0  0<br>  5 75  1  0  0  0  0<br>  6 22  1  0  0  0  0<br>  6 32  1  0  0  0  0<br>  6 76  1  0  0  0  0<br>  7 33  1  0  0  0  0<br>  7 35  1  0  0  0  0<br>  7 89  1  0  0  0  0<br>  8 34  1  0  0  0  0<br>  8 36  1  0  0  0  0<br>  8 90  1  0  0  0  0<br>  9 15  1  0  0  0  0<br>  9 37  1  0  0  0  0<br>  9 38  1  0  0  0  0<br> 10 16  1  0  0  0  0<br> 10 39  1  0  0  0  0<br> 10 40  1  0  0  0  0<br> 11 17  1  0  0  0  0<br> 11 41  1  0  0  0  0<br> 11 42  1  0  0  0  0<br> 12 18  1  0  0  0  0<br> 12 43  1  0  0  0  0<br> 12 44  1  0  0  0  0<br> 13 19  1  0  0  0  0<br> 13 45  1  0  0  0  0<br> 13 46  1  0  0  0  0<br> 14 20  1  0  0  0  0<br> 14 47  1  0  0  0  0<br> 14 48  1  0  0  0  0<br> 15 21  1  0  0  0  0<br> 15 49  1  0  0  0  0<br> 15 50  1  0  0  0  0<br> 16 22  1  0  0  0  0<br> 16 51  1  0  0  0  0<br> 16 52  1  0  0  0  0<br> 17 23  2  0  0  0  0<br> 17 25  1  0  0  0  0<br> 18 24  2  0  0  0  0<br> 18 26  1  0  0  0  0<br> 19 53  1  0  0  0  0<br> 19 54  1  0  0  0  0<br> 20 55  1  0  0  0  0<br> 20 56  1  0  0  0  0<br> 21 57  1  0  0  0  0<br> 21 58  1  0  0  0  0<br> 22 59  1  0  0  0  0<br> 22 60  1  0  0  0  0<br> 23 24  1  0  0  0  0<br> 23 61  1  0  0  0  0<br> 24 62  1  0  0  0  0<br> 25 26  2  0  0  0  0<br> 25 63  1  0  0  0  0<br> 26 64  1  0  0  0  0<br> 27 29  1  0  0  0  0<br> 27 67  1  0  0  0  0<br> 27 68  1  0  0  0  0<br> 28 30  1  0  0  0  0<br> 28 69  1  0  0  0  0<br> 28 70  1  0  0  0  0<br> 29 33  1  0  0  0  0<br> 29 71  1  0  0  0  0<br> 29 72  1  0  0  0  0<br> 30 34  1  0  0  0  0<br> 30 73  1  0  0  0  0<br> 30 74  1  0  0  0  0<br> 31 35  1  0  0  0  0<br> 31 77  1  0  0  0  0<br> 31 78  1  0  0  0  0<br> 32 36  1  0  0  0  0<br> 32 79  1  0  0  0  0<br> 32 80  1  0  0  0  0<br> 33 81  1  0  0  0  0<br> 33 82  1  0  0  0  0<br> 34 83  1  0  0  0  0<br> 34 84  1  0  0  0  0<br> 35 85  1  0  0  0  0<br> 35 86  1  0  0  0  0<br> 36 87  1  0  0  0  0<br> 36 88  1  0  0  0  0<br>M  END
Compound Name

Plerixafor

CID

65015

Molecular Formula

C28H54N8

Molecular Weight

502

No. Hydrogen Bond Acceptors

8

No. Hydrogen Bond Donors

6

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