| 1Chloroacetic acid |
|---|
| 2Bromoacetic acid |
| 3Dichloroacetic acid |
| 4Dalapon |
| 5Trichloroacetic acid |
| 6Bromochloroacetic acid |
| 71,2,3-Trichloropropane |
| 8Dibromoacetic acid |
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Applications
EPA 552.1 by Strata-X-A on a ZB-XLB-HT
19322
Separation Mode: High Temperature
High Temperature
EPA 552
ZB-XLB-HT
GC
Caustics
Pollutant / Contaminant
Environmental / Health
Analytes
Details
Official Method: EPA 552
GC Conditions (App ID: 19322)
Column: |
Part No: |
Phase Name: ZB-XLB-HT |
Sample Notes: Derivatization: Add 1mL of MTBE to the eluent in a screw cap vial or test tube. Heat the sample at 50ºC for 1.5 hours. Remove and allow the sample to cool to room temperature. Slowly add 10mL of saturated sodium bicarbonate and invert the sample several times releasing carbon dioxide gas frequently. Aspirate 100µL of the organic layer and transfer to a 2mL vial with insert. Add 10µL of internal standard (1,2,3-Trichloropropane) and inject into GC-ECD system. |
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