Column:
Zebron ZB-1
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Dimension:
10 meter x 0.53 mm x 2.65 µm
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Part No.:
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Injection Volume:
Split 10:1 @ 360 °C, 1 µL* |
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Carrier Gas:
Helium @ 8.1 mL/min (constant flow) |
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Oven Program:
35 °C to 360 °C @ 15 °C/min for 5 min |
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Detection:
FID @ 360 °C |
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Samples:
1. Pentane (C5)
2. Hexane (C6)
3. Heptane (C7)
4. Octane (C8)
5. Nonane (C9)
6. Decane (C10)
7. Undecane (C11)
8. Dodecane (C12)
9. Tetradecane (C14)
10. Pentadecane (C15)
11. Hexadecane (C16)
12. Heptadecane (C17)
13. Octadecane (C18)
14. Eicosane (C20)
15. Tetracosane (C24)
16. Octacosane (C28)
17. Dotriacontane (C32)
18. Hexatriacontane (C36)
19. Tetracontane (C40)
20. Tetratetracontane (C44) |
Column:
Zebron ZB-1
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Phase:
100% Dimethylpolysiloxane
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Dimension:
30 meter x 0.32 mm x 3.00 µm
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Part No.:
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Injection Volume:
Split 10:1 @ 270 °C, 1 μL |
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Carrier Gas:
Helium @ 2 mL/min (constant flow) |
Oven Program:
50 °C for 1 min to 300 °C @ 10 °C/min for 3 min
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Detection:
Sulfur (SCD) @ 320 °C
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Analytes:
1. Thiophene
2. Dimethyldisulfide
3. 2-Methyl-thiophene
4. 3-Methyl-thiophene
5. C2-Thiophenes
6. Diethylsulfide
7. Dibutylsulfide
8. Benzothiophene
9. C1-Benzothiophenes
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